Method for producing a polycarbonate oligomer
AssigneeIdemitsu Petrochemical Co., Ltd.
InventorsIchiro Tokumitsu, Hideo Konuma, Shigeaki Mochizuki, Kohichi Morotomi, Norio Murai, Mikio Koyama
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Abstract
Polycarbonate oligomer having uniform qualities is prepared by reacting an aqueous alkaline solution of 2,2-(4,4'-dihydroxydiphenyl) propane with phosgene in the presence of methylene chloride and as a characteristic point of this method, in the presence of an inert gas in an amount of 1 to 10 mol % based upon the phosgene.
Claims3
In the method for producing polycarbonate oligomers having an average molecular weight of 430-460 and a chloroformate radical concentration of 1.1 to 1.2 mol per liter of methylene chloride solution by introducing an aqueous alkaline solution of 2,2-(4,4'-dihydroxy-diphenyl) propane and methylene chloride into a tubular type reactor to form a mixed phase stream which is reacted with phosgene in a parallel flow, the improvement which comprises introducing one to 10 mol % of an inert gas based upon phosgene, together with phosgene into said tubular type reactor.
Dependencies are inferred from the claim text.