Microwave drying process for synthetic polymers
AssigneeExxon Research & Engineering Co.
InventorsEric O. Forster, Peter J. Creighton
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AssigneeExxon Research & Engineering Co.
InventorsEric O. Forster, Peter J. Creighton
Estimating the term…
Volatile polar vehicles such as water or organic solvents, are removed from nonpolar materials by passing said material through at least one pneumatic conveyor resonating cavity operating at a microwave frequency of about 600 to about 50,000 MHZ. For example, a polymer such as polyvinyl chloride may be dried by conveying the polymer through said pneumatic conveyor operating at a frequency of 915 MHZ for a time sufficient to reduce the volatiles content to about 5 wt. % and subsequently conveying the partially dried material through a second pneumatic conveyor resonating cavity operating at a microwave frequency of 2450 MHZ for a time sufficient to reduce the polar vehicle content to below 0.5 wt. %. The resonating cavities may constitute a single pneumatic conveyor having zones operating at different frequencies, said zones being isolated from one another by microwave suppressors such as "eggcrate" type suppressors. Alternately, several pneumatic conveyor systems, each operating at a different frequency, may be used.
In a process for preparing butyl rubber wherein a slurry of said rubber is formed in a diluent from which said rubber is separated by introducing said slurry into water, thereby forming a water slurry of butyl rubber, the steps which comprise:
Dependencies are inferred from the claim text.