Non-frangible alumina-silica fibers
AssigneeMinnesota Mining and Manufacturing Company
InventorsKarl A. Karst, Harold G. Sowman
Life of this patent
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Abstract
Transparent, smooth, fracture resistant, discreet, refractory oxide fibers of homogeneous chemical composition comprising 96 to 100 weight percent of a mixture or chemical combination of 67 to 77 parts by weight alumina and 23 to 33 parts by weight silica, said fibers having a predominant polycrystalline phase of mullite, transitional alumina, or a mixture of both, said refractory fibers being made by fiberizing a viscous liquid of oxide precursors comprising a silica sol and a water dispersible alumina sol or water soluble or dispersible organic aluminum salt, and drying, collecting, and calcining the resulting green fibers.
Claims23
Transparent, smooth, fracture resistant, discrete, refractory oxide fibers uniformly round in cross section and of homogenous chemical composition comprising 96 to 100 weight percent of a mixture or chemical combination of 67 to 77 parts by weight alumina and 23 to 33 parts by weight silica, and fibers having a predominant polycrystalline phase of mullite, transitional alumina, or a mixture of both.
Transparent, smooth, discrete, continuous, refractory, ceramic oxide fibers of homogeneous chemical composition comprising 99 to 99.5 weight percent of a mixture or chemical combination of 70 to 75 parts by weight alumina and 25 to 30 parts by weight silica, 0.5 to 1 weight percent of boria or phosphorus pentoxide, or both, and less than 0.1 weight percent carbon, said fibers being free of alpha alumina and having a polycrystalline phase of predominantly transitional alumina in admixture with silica which admixture is transformable upon firing said fibers at 1200.degree. to 1400.degree. C to mullite crystallites, said fibers having a friability index of at least 0.5 and a surface area less than 1 m.sup.2 /g, said fibers being straight and uniformly round with a uniform diameter of 7 to 15 micrometers.
Transparent, smooth, fracture resistant, discrete, refractory oxide fibers uniformly round in cross-section and of homogeneous chemical composition comprising 96 to 100 weight percent of a mixture or chemical combination of 67 to 77 parts by weight alumina and 23 to 33 parts by weight silica, said fibers having a predominant polycrystalline phase of mullite, transitional alumina, or a mixture of both, a friability index of at least 0.2 and a surface area of less than 1 m.sup.2 /g.
Dependencies are inferred from the claim text.