US 4,030,966 AGranted

Method of hydrothermally growing quartz

AssigneeWestern Electric Company, Inc.

InventorsCarl F. Hornig, Kenneth M. Kroupa, Earle E. Simpson

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Abstract

This invention relates to a method of growing a single quartz crystal stone. In particular, a method for hydrothermally growing a quartz stone from a quartz seed is disclosed. A substantially stress-free quartz stone is grown in an autoclave by clamping a quartz crystal seed plate in a clip so as to permit substantially unobstructed growth of the stone in the plane of the seed plate, and growing at least a portion of the stone through at least one aperture formed in the clip.

Claims2

Dependent claims

In a method of hydrothermally growing a substantially stress-free quartz crystal from a planar quartz crystal seed plate having first and second major faces on opposite sides thereof, in which at least a portion of the seed plate adjacent one edge is inserted into and clamped in a supporting clip, and in which the seed plate is of a type which grows in thickness perpendicular to the plane of the seed plate, and in length and width from respective edges thereof in respective directions in the plane of the seed plate, the improvement which comprises the steps of:

clamping the major faces of the seed plate between first and second clamping fingers projecting from a body portion of the supporting clip, with each clamping finger engaging a respective one of the faces, at least one of the clamping fingers having a stress-relieving aperture formed therethrough of a small cross-sectional area in comparison to the cross-sectional area of the clamping finger and at least one of the clamping fingers including a projecting stop spaced from junctions of the first and second clamping fingers with the body portion, the stress-relieving aperture being essentially positioned intermediate the stop and a seed plate engaging end of the supporting clip;
limiting the extent to which the portion of the seed plate is inserted into the supporting clip between the first and second clamping fingers by engaging the one edge of the seed plate with the projecting stop so that the edge is spaced from the junctions of the first and second clamping fingers with the body portion of the supporting clip to permit substantially unobstructed stress-free growth of the quartz crystal from the edge in its respective direction in the plane of the seed plate;
and
hydrothermally growing a portion of the major face of the quartz crystal seed plate which is engaged by the clamping finger having the stress-relieving aperture, through the stress-relieving aperture in the clamping finger in a direction perpendicular to the plane of the seed plate to reduce stress-cracking of the quartz crystal during the hydrothermal growing thereof.

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Dependencies are inferred from the claim text.

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Abstract

clamping the major faces of the seed plate between first and second clamping fingers projecting from a body portion of the supporting clip, with each clamping finger engaging a respective one of the faces, at least one of the clamping fingers having a stress-relieving aperture formed therethrough of a small cross-sectional area in comparison to the cross-sectional area of the clamping finger and at least one of the clamping fingers including a projecting stop spaced from junctions of the first and second clamping fingers with the body portion, the stress-relieving aperture being essentially positioned intermediate the stop and a seed plate engaging end of the supporting clip;
limiting the extent to which the portion of the seed plate is inserted into the supporting clip between the first and second clamping fingers by engaging the one edge of the seed plate with the projecting stop so that the edge is spaced from the junctions of the first and second clamping fingers with the body portion of the supporting clip to permit substantially unobstructed stress-free growth of the quartz crystal from the edge in its respective direction in the plane of the seed plate;
and
hydrothermally growing a portion of the major face of the quartz crystal seed plate which is engaged by the clamping finger having the stress-relieving aperture, through the stress-relieving aperture in the clamping finger in a direction perpendicular to the plane of the seed plate to reduce stress-cracking of the quartz crystal during the hydrothermal growing thereof.

1 more element