Anionic dyeing of novoloid fibers
AssigneeThe Carborundum Company
InventorsJames Economy, George Y. Lei
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Abstract
Compositions are disclosed for dyeing cross-linked novolac fibers, and blends thereof, using anionic dyes and premetallized dyes.
Claims19
A composition for dyeing novoloid fibers, said composition comprising
- 1. from about 1 to about 10 percent anionic dye based upon fiber weight,
- 2. from about 3 to about 10 volume percent carrier medium selected from the group consisting of benzyl alcohol and benzyl alcohol/acetophenone,
- 3. from about 1 to about 10 volume percent formic acid,
- 4. from about 1 to about 5 volume percent acetic acid,
- 5. a small amount, less than 0.1 weight percent of surface active agent, and
- 6. water.
A dye bath comprising:
- 1. from 5 to 7.5 percent anionic dye, based on weight of fiber to be dyed;
- 2. from about 5 to about 6 volume percent of benzyl alcohol;
- 3. from about 1 to about 5 volume percent formic acid;
- 4. from about 1 to about 2 volume percent acetic acid;
- 5. a small amount, less than 0.1 weight percent of surface active agent, and
- 6. water.
A dye bath comprising:
- 1. from 5 to 7.5 percent premetallized dye, based on weight of fiber to be dyed;
- 2. from about 5 to about 6 volume percent benzyl alcohol/acetophenone;
- 3. from about 1 to about 5 volume percent formic acid;
- 4. from about 1 to about 2 volume percent acetic acid;
- 5. a small amount, less than 0.1 weight percent of surface active agent, and
- 6. water.
An anionic-dyed novoloid fiber.
An anionic-dyed infusible phenolic resin fiber having at least 50 percent of the phenolic hydroxyl groups blocked by esterification.
An anionic-dyed fiber comprising a novoloid resin and an aromatic polyamide.
A composition for dyeing novoloid fibers, said composition comprising, per liter,
- 1. from about 1/3 to about 31/3 grams anionic dye;
- 2. from about 30 to about 100 milliliters carrier medium selected from the group consisting of benzyl alcohol and benzyl alcohol/acetophenone;
- 3. from about 10 to about 100 milliliters formic acid;
- 4. from about 10 to about 50 milliliters acetic acid;
- 5. a small amount, less than 0.1 weight percent of surface active agent, and
- 6. water.
A dye bath comprising, per liter:
- 1. from 12/3 to 21/2 grams anionic dye;
- 2. from about 50 to about 60 milliliters of benzyl alcohol;
- 3. from about 10 to about 50 milliliters formic acid;
- 4. from about 10 to about 20 milliliters acetic acid;
- 5. a small amount, less than 0.1 weight percent of surface active agent, and
- 6. water.
A dye bath comprising, per liter:
- 1. from 12/3 to 21/2 grams premetallized dye;
- 2. from about 50 to about 60 milliliters volume percent benzyl alcohol/acetophenone;
- 3. from about 10 to about 50 milliliters formic acid;
- 4. from about 10 to about 20 milliliters acetic acid;
- 5. a small amount, less than 0.1 weight percent or surface active agent, and
- 6. water.
Dependencies are inferred from the claim text.