Concentrating vortex shaker
AssigneeBuchler Instruments, Div. of Searle Analytic, Inc.
InventorsBernard Parker, Otto Gross, Joseph Buchler
Life of this patent
Estimating the term…
Abstract
A concentrating vortex shaker for the simultaneous shaking and concentration of a multiplicity of liquid samples comprises a heat-conductive block having a plurality of openings for receiving laboratory vessels containing sample liquids and removably mounted on a base provided with an adjustable eccentric drive for displacing the block in a gyrating motion. An airtight cover is removably mounted on the block and forms a chamber above the samples which can be controllably evacuated. The samples can be heated or cooled by a temperature-controlled liquid which is fed through a channel formed in the block or heated by an adjustable electrical heater provided in the block mounting or cooled by a cooling plate, upon which the block mounts.
Claims11
a shaker apparatus, comprising:
- a base;
- a heat-conductive block movably mounted on said base;
- drive means on said base for displacing said block in gyrating motion;
- said block having a plurality of openings for receiving sample vessels;
- an airtight cover on said block, overlying said openings and forming a chamber above said block;
- suction means for creating a vacuum in said chamber;
- and
- control means for adjusting the temperature of said block, said control means for adjusting the temperature of said block comprising:
- a heater assembly carrying and in contact with said block, said heater assembly being provided with a resistance-type heater and a temperature sensor;
- and
- a control connected with said heater and said sensor for adjusting the temperature of said assembly.
A shaker apparatus, comprising:
- a base;
- a heat-conductive block movably mounted on said base;
- drive means on said base for displacing said block in gyrating motion;
- a plurality of openings formed in said block for receiving sample vessels;
- an airtight cover on said block, overlying said openings and forming a chamber above said block;
- suction means for creating a vacuum in said chamber;
- and
- control means for adjusting the temperature of said block, said suction means comprising:
- a passageway formed in said block and communicating between said chamber and a vacuum source;
- and
- means for adjusting and monitoring the rate at which a vacuum is created in said chamber, said adjusting and monitoring means comprising:
- a duct communicating between said chamber and said vacuum source;
- a first solenoid valve normally closed for controlling the flow of air in said duct between said chamber and said vacuum source;
- a second solenoid valve normally open for feeding atmosphere air to said duct between said first solenoid valve and said vacuum source;
- a nozzle in said duct for limitedly feeding a flow of air past said first solenoid valve;
- means for energizing said vacuum source and said second solenoid valve into a closed position simultaneously;
- means responsive to a predetermined level of air pressure in said duct between said chamber and said first solenoid valve for energizing said first solenoid valve into an open position;
- and
- a vacuum gauge communicating with said duct between said first solenoid valve and said chamber.
A shaker apparatus, comprising:
- a base;
- a heat-conductive block movably mounted on said base;
- drive means on said base for displacing said block in gyrating motion;
- a plurality of openings formed in said block for receiving sample vessels;
- an airtight cover on said block, overlying said openings and forming a chamber above said block;
- suction means for creating a vaccum in said chamber;
- and
- control means for adjusting the temperature of said block, said control means including a heater assembly carrying said block;
- said block being removably mounted on said heater assembly by a single removable central fastening member provided with a manually-grippable top;
- and
- an indexing pin provided on said heater assembly and engageable with said block for orientation thereof.
A shaker apparatus, comprising:
- a base;
- a heat-conductive block movably mounted on said base;
- drive means on said base for displacing said block in gyrating motion;
- a plurality of openings formed in said block for receiving sample vessels;
- an airtight cover on said block, overlying said openings and forming a chamber above said block;
- suction means for creating a vacuum in said chamber;
- and
- control means for adjusting the temperature of said block, said drive means including a drive shaft journaled on said base and rotated by a motor;
- a mounting plate removably carrying said block;
- an eccentric fixed to said drive shaft and rotatably supporting said mounting plate;
- a plurality of springs connected with said mounting plate and said base for resiliently biasing said plate against rotation;
- a counterweight fixed to said eccentric for dynamically balancing said block;
- and
- a control for adjusting the speed of said motor;
- said control means for adjusting the temperature of said block comprises:
- a channel formed in said heat-conductive block;
- means for feeding a temperature-controlled liquid through said channel;
- a heater assembly carrying and in contact with said block, said heater assembly being provided with a resistance-type heater and a temperature sensor;
- and
- a control connected with said heater and said sensor for adjusting the temperature of said assembly;
- said suction means comprises:
- a passageway formed in said block and communicating between said chamber and a vacuum source;
- a valve between said passageway and said vacuum source for adjusting the rate at which a vacuum is created in said chamber;
- a vacuum gauge between said valve and said chamber for monitoring a vacuum created in said chamber;
- said cover is removably attached on said block by catches provided on said block;
- said cover is transparent;
- said block is removably mounted on said heater assembly by a single removable central fastening member provided with a manually-grippable top;
- and
- an indexing pin is provided on said heater assembly and engageable with said block for orientation thereof.
A vortex shaker comprising:
- a base;
- a motor in said base;
- a heat-conductive block mounted movably on said base and connected to said motor for gyratory movement of said block by said motor, said block being formed with a plurality of upwardly open pockets adapted to receive sample vessels;
- means for selectively heating and cooling said block to vary the temperature thereof;
- a cover detachably engaging said block and enclosing said pockets while forming a hermetic seal with said block while defining a chamber above said pockets common to all said pockets;
- suction means communicating with said chamber for inducing a suction therein;
- and
- control means connected to said suction means for regulating the generation of suction in said chamber to prevent bumping of said liquid in said vessels.
Dependencies are inferred from the claim text.