Method for recycling iron ions and preparing iron(iii) phosphate
AssigneeHydroionic Technologies Co., Ltd.
InventorShun-Hsuan WU
Life of this patent
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Abstract
A method for recycling iron ions and preparing FePO4 is provided. The method includes: (a) providing an iron ion-containing solution; (b) passing the iron ion-containing solution through a chelating cation exchange resin to obtain an ion-adsorbed resin and a first eluate; (c) desorbing ferric ions from the ion-adsorbed resin using a phosphoric acid solution with a concentration ranging from 10 wt % to 45 wt %, producing an ion-desorbed resin and a second eluate; and (d) heating the second eluate to produce a third solution containing an FePO4 precipitate. This method efficiently recycles iron ions, prepares FePO4 with minimal waste, and reduces overall costs.
Claims20
A method for recycling iron ions and preparing iron(III) phosphate, comprising the following steps:
- Step (a):
- Providing an iron ion-containing solution, wherein, the iron ion-containing solution comprises an iron chloride solution, an iron sulfate solution or a combination thereof,
- Step (b):
- Passing the iron ion-containing solution through a chelating cation exchange resin capable of adsorbing ferric ions to obtain an ion-adsorbed resin and a first eluate;
- Step (c):
- Passing a phosphoric acid solution through the ion-adsorbed resin to desorb ferric ions, thereby obtaining an ion-desorbed resin and a second eluate, wherein the second eluate comprises ferric ions and phosphate ions, and the phosphoric acid solution has a concentration ranging from 10 weight percent to 45 weight percent;
- and
- Step (d):
- Heating the second eluate to obtain a third solution, wherein the third solution comprises an iron(III) phosphate precipitate.
Dependencies are inferred from the claim text.