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US 2026/0158484 A1Published application
Method for treating a catalyst
AssigneeEvonik Oxeno GmbH
InventorsRobert Franke, Thomas Quandt, Johannes Knossalla
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Abstract
A method for treating a catalyst may involve a hydrothermal treatment step in which the drying rate is lower than the drying rate in the subsequent drying step. The catalyst can be treated according to this method, before its first use, preferably in oligomerization, or after its use, preferably in oligomerization.
Claims15
1-14. (canceled)
A process for treatment of a nickel-containing catalyst, the process comprising at least:
- a) thermally treating the nickel-containing catalyst at a temperature of 500° C. to 900° C. to remove carbon-containing deposits;
- b) impregnating the nickel-containing catalyst with an aqueous or ammoniacal solution comprising a nickel compound;
- c) hydrothermally treating the nickel-containing catalyst, wherein the hydrothermal treatment is carried out in that the nickel-containing catalyst is heated from room temperature to a temperature in a range from 75° C. to 150° C. and optionally held at the temperature until a residual moisture content of not more than 30% is obtained, wherein the hydrothermal treatment is carried out at a pressure higher than atmospheric pressure;
- d) drying of the nickel-containing catalyst, wherein a drying rate in the drying in d) is higher than in the hydrothermal treatment in c) and wherein the drying is carried out to a residual moisture content of not more than 15%;
- and
- e) calcinating the catalyst.
3 more elements
Dependencies are inferred from the claim text.