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US 2026/0146058 A1Published application
Alternative allulose crystal process
AssigneeTate & Lyle Solutions USA LLC
InventorKrishnan Viswanathan Iyer
Life of this patent
Estimating the term…
Abstract
Allulose crystals are efficiently produced from an allulose syrup using seed crystals.
Claims38
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An allulose crystal product having a mean particle size of from 100 to 500 microns and a d10 of from 10-100 microns on a volume basis as measured by laser diffraction;
- and/or having a d90 of from 300-1000 microns on a volume basis as measured by laser diffraction;
- and/or having a median particle size of from 50-250 microns on a volume basis as measured by laser diffraction;
- and/or having a bulk density of at least 30 lb/ft3.
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A method for producing allulose crystals, wherein the method comprises:
- a) evaporating a feed allulose syrup at a sub-ambient pressure and a first temperature to produce a first supersaturated allulose syrup having an allulose syrup target saturation;
- b) introducing seed crystals to the first supersaturated allulose syrup and allowing the allulose to crystallize at a crystallization rate to produce a first massecuite comprising allulose crystals and a first supersaturated mother liquor having a first target mother liquor saturation higher than the allulose syrup target saturation;
- c) evaporating the first massecuite at the sub-ambient pressure and a second temperature, lower than the first temperature to produce a second massecuite comprising allulose crystals and a second supersaturated mother liquor having a second mother liquor target saturation lower than the first mother liquor target saturation;
- d) increasing the pressure to ambient and cooling the second massecuite to a third temperature lower than the second temperature at a cooling rate to produce a third massecuite comprising allulose crystals and a third supersaturated mother liquor having a third target mother liquor saturation;
- e) allowing the third massecuite to crystallize for a crystallization time to produce a product massecuite comprising product allulose crystals at a target yield and a product mother liquor, the product mother liquor having a target product mother liquor supersaturation;
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- f) separating the product allulose crystals from the product supersaturated mother liquor to provide allulose crystals at the target yield.
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Dependencies are inferred from the claim text.