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US 2026/0132224 A1Published application
Method for producing silylated cellulose
OwnerBeata Kilos, Marc-Andre Courtemanche +4inventors
InventorsBeata Kilos, Marc-Andre Courtemanche, Matthew McLaughlin, Michael Telgenhoff, David Williams, Ryan Baumgartner
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Abstract
A method for preparing silylated cellulose is disclosed. The method includes preparing a reaction product in the form of a paste and removing unreacted starting materials and/or by-products from the paste to form a powdered silylated cellulose.
Claims14
A method for preparing a silylated cellulose, wherein the method comprises:
- 1) combining starting materials comprising
- A) a cellulose comprising repeating monomeric units and having >2.5 to 3 hydroxyl groups per monomeric unit,
- B) a polar aprotic swelling agent,
- C) a catalyst, and
- D) a silylating agent comprising a silyl amine having a silicon-nitrogen moiety,
- thereby forming a reaction mixture;
- and
- 2) mixing the reaction mixture in a reactor with self-wiping mixing blades, and heating the reaction mixture at a temperature of 30° C. to 150° C., thereby forming a reaction product comprising the silylated cellulose with a degree of substitution>2, and where the starting materials are used in amounts such that the reaction mixture or the reaction product is a paste.
5 more elements
Dependencies are inferred from the claim text.