Method of preparing black phosphorus crystals

Abstract

Provided is a method of preparing black phosphorus crystal. First, one area of a double-opening reactor is used as the feedstock area, the other area is used as the nucleation area, and the middle area is used as a transition section, and the feedstock area is sealed, the phosphorus feedstock and the transport agent are weighed and placed inside the feedstock area under an inert atmosphere, then the nucleation area is sealed, the first step of heating reaction is performed in the reactor through an optimized temperature-control program, when the reaction is complete, monoclinic phosphorus crystals are prepared in the feedstock area. Then the nucleation area of the reactor is started, the weighed catalyst is placed inside the feedstock area under an inert atmosphere, and the nucleation area is sealed, and then the second step of a heating reaction is performed in the reactor through an optimized temperature-control program.

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