Dithiolate-based compounds
AssigneeThe Government of the United States of America, as represented by the Secretary of the Navy
InventorsEunkeu Oh, Kimihiro Susumu, Scott A. Walper, Jozsef Czege
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Abstract
The compounds shown below are presented. The compounds have a bidentate binding group: thioctic acid (TA) with disulfide or its reduced form of dihydrolipoic acid (DHLA) with dithiol. In embodiments, the compounds form part of a dithiolate-based ligand-grafted gold nanoparticle (AuNP). A method includes: mixing a testing material with a dithiolate-based ligand-grafted AuNP probe in solution, thereby generating a test sample; chilling the test sample at a predetermined temperature for a period of time; subsequent to chilling the test sample, detecting a color of the test sample; and determining anti-icing effects of the testing material based on the color of the test sample.
Claims4
A compound having the formula:
A compound having the formula:
A method comprising:
- reacting 2-[2-(2-chloroethoxy)ethoxy]ethanol with N-(tert-butoxycarbonyl)ethylenediamine to form N,N-bis{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}-N′-(tert-butoxycarbonyl)ethylenediamine;
- treating the N,N-bis{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}-N′-(tert-butoxycarbonyl)ethylenediamine with acid to form N,N-bis{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethylenediamine;
- reacting the N,N-bis{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethylenediamine with thioctic acid to form the product:
Dependencies are inferred from the claim text.