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US 2025/0109482 A1Published application
Formation apparatus and method of hydroxyapatite-containing thin film
AssigneeBrainy Inc.
InventorsNobukiyo Tanaka, Masashi Tanaka
Life of this patent
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Abstract
A formation apparatus of a hydroxyapatite-containing thin film includes a sputtering device which forms a thin film of a material including an antibacterial metal and hydroxyapatite on a surface of an object by sputtering, and a hydrothermal treatment device which performs hydrothermal treatment on the object, on which the thin film is formed, using an alkaline solution.
Claims5
A formation apparatus of a hydroxyapatite-containing thin film, the formation apparatus comprising:
- a sputtering device which forms a thin film of a material including an antibacterial metal and hydroxyapatite on a surface of an object by sputtering, the object being an artificial joint or a dental implant;
- a hydrothermal treatment device which performs hydrothermal treatment on the object, on which the thin film is formed, using an alkaline solution;
- a first control device which controls the sputtering device;
- and
- a second control device which controls the hydrothermal treatment device,
- the sputtering device comprising:
- a first container;
- a holder provided in the first container and used to place the object, on which the thin film is yet to be formed, on a first surface;
- an electrode provided in the first container, including a second surface facing the first surface of the holder, and used to place the material on the second surface;
- and
- an inert gas filling device which fills the first container with an inert gas,
- the first control device switching a positive pole and a negative pole of the electrode at a predetermined frequency or higher, controlling the inert gas filling device to control a pressure in the first container, and controlling the sputtering device to make an atomic number ratio (calcium/phosphorus) of calcium to phosphorus in the thin film range from 1.0 to 3.0 and to make a thickness of the thin film range from 0.1 μm to 10 μm,
- the hydrothermal treatment device comprising a second container which accommodates the object, on which the thin film is formed by the sputtering device,
- the second control device performing the hydrothermal treatment, with the thin film at a temperature of 100° C. to 180° C., using the alkaline solution with a pH of 9 to 11, and adjusting a pressure in the second container by changing the temperature during the hydrothermal treatment.
11 more elements
A formation method of a hydroxyapatite-containing thin film, the formation method comprising:
- forming a thin film of a material including an antibacterial metal and hydroxyapatite on a surface of an object by sputtering, the object being an artificial joint or a dental implant;
- and
- performing hydrothermal treatment on the object, on which the thin film is formed, using an alkaline solution,
- the sputtering comprising:
- providing the object, on which the thin film is yet to be formed, on a first surface of a holder in a first container, and providing the material on a second surface of an electrode facing the first surface of the holder in the first container;
- filling the first container with an inert gas;
- and
- switching a positive pole and a negative pole of the electrode at a predetermined frequency or higher, controlling the filling with the inert gas to control a pressure in the first container, and forming the thin film on the object to make an atomic number ratio (calcium/phosphorus) of calcium to phosphorus in the thin film range from 1.0 to 3.0 and to make a thickness of the thin film range from 0.1 μm to 10 μm,
- the hydrothermal treatment comprising:
- accommodating the object, on which the thin film is formed by the sputtering, in a second container;
- and
- using the alkaline solution with a pH of 9 to 11, with the thin film at a temperature of 100° C. to 180° C., and adjusting a pressure in the second container by changing the temperature.
9 more elements
Dependencies are inferred from the claim text.