Preparation method for iron phosphate and preparation method for lithium iron phosphate
AssigneeHubei Yuhao High-Tech New Material Co., Ltd.
InventorQin WANG
Life of this patent
Estimating the term…
Abstract
In one aspect, a preparation method of iron phosphate includes: mixing pyrite cinder and an sulfite evenly in water to obtain a first mixed system; adding phosphoric acid and a buffer to the first mixed system to perform a leaching reaction; performing a first solid-liquid separation on a slurry obtained from the leaching reaction to obtain a first filtrate and a first residue; introducing air into the first filtrate and then performing a first stirring reaction on the first filtrate; performing a second solid-liquid separation on a slurry obtained from the first stirring reaction to obtain a second filtrate and a second residue; and calcining the second residue to obtain iron phosphate.
Claims21
1-10. (canceled)
A preparation method of iron phosphate, comprising:
- mixing pyrite cinder and a sulfite evenly in water to obtain a first mixed system;
- adding phosphoric acid and a buffer to the first mixed system to perform a leaching reaction;
- performing a first solid-liquid separation on a slurry obtained from the leaching reaction to obtain a first filtrate and a first residue;
- introducing air into the first filtrate and then performing a first stirring reaction on the first filtrate;
- performing a second solid-liquid separation on a slurry obtained from the first stirring reaction to obtain a second filtrate and a second residue;
- and
- calcining the second residue to obtain iron phosphate;
- wherein the leaching reaction is performed at a pressure of 0.25 MPa˜0.5 MPa for a time of 1 hour˜2 hours;
- a pH of a reaction system of the leaching reaction is 1.5˜3;
- the buffer comprises sodium dihydrogen phosphate and/or disodium hydrogen phosphate.
Dependencies are inferred from the claim text.