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US 2025/0018599 A1Published application
Process and slip for the production of ceramic shaped bodies made of zirconium oxide by 3d inkjet printing
AssigneeIvoclar Vivadent AG
InventorsChristian Ritzberger, Johannes Renner
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Abstract
Process and slip for the production of ceramic shaped parts made of zirconium oxide ceramic by a 3D inkjet printing process. The slip contains zirconium oxide which is suspended in a liquid medium, wherein the slip has a zirconium oxide content of from 68 to 88 wt.-% and contains not more than 5 wt.-% organic components. The process for the production of ceramic components comprises the layered shaping and subsequent sintering of the desired component from the slip.
Claims15
A process for the production of a ceramic shaped part by an inkjet printing process, comprising
- (i) shaping a slip in layers into a geometric shape of the desired ceramic shaped part, wherein the individual layers are each dried after printing to produce a green compact,
- (ii) optionally drying the green compact,
- (iii) applying a staining solution to the green body, and
- (iv) sintering the green compact,
- wherein the layered construction of the green compact in step (i) is effected by a layered inkjet printing process,
- wherein the slip comprises zirconium oxide with a particle size of from 50 to 250 nm, measured as the d50 value and relative to the volume of the particles, suspended in a liquid medium, and has a zirconium oxide content of from 68 to 88 wt.-%, and not more than 3 wt.-% organic components, relative to the total mass of the slip,
- wherein the slip has a viscosity of 5 to 100 mPas, measured at a shear rate of from 0.1 to 1000 s-1 and at a temperature of 25° C., and
- wherein the printed ceramic shaped part is sintered directly after printing and optionally subsequent drying without a separate debinding step.
5 more elements
A green body comprising
- a density of from 3.3 to 4.0 g/cm3, and/or
- a pore volume of from 0.08 to 0.14 cm3/g and/or
- a pore diameter of from 0.02 to 0.12 μm measured as the d50 value relative to the volume of the particles.
Dependencies are inferred from the claim text.