Synthetic method and catalyst of 3-(3-oxo-2-pentyl)cyclopentyl dimethyl malonate

Abstract

A synthetic method and catalyst for preparing 3-(3-oxo-2-pentyl)cyclopentyl dimethyl malonate are disclosed. The synthetic method uses 2-pentyl-2-cyclopentenone and dimethyl malonate as raw materials, and reacts them in the presence of a catalyst to prepare 3-(3-oxo-2-pentyl)cyclopentyl dimethyl malonate, the catalyst is a basic ionic liquid, the pH value of the basic ionic liquid is greater than or equal to 10, and the catalyst is prepared by a method comprising the steps of: mixing the nitrogen-containing heterocyclic compound with an aliphatic carboxylate or hydroxyl aliphatic carboxylate or fluorophosphate under stirring. The synthetic method is environmentally friendly, stable in reaction and low-cost, and the conversion of 2-pentyl-2-cyclopentenone is significantly improved due to the use of the above-mentioned basic ionic liquid as catalyst.

Dependencies are inferred from the claim text.