Method of preparing alkali-activated cement by stepwise calcination with sodium chloride
AssigneesHunan University of Science and Technology, Hunan Xiangchu Xianlu Environmental Protection Technology Co., Ltd.
InventorsMeixun PENG, Qiming ZHAO, Yuanpeng ZHANG, Wenwei LIU, Meilin CHEN
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Abstract
A method of preparing alkali-activated cement by stepwise calcination with sodium chloride includes the following steps. (1) Sodium chloride, a silicate and a carbonate are mixed and finely ground to obtain a raw material powder. (2) The raw material powder is calcined sequentially at 850-1050° C. and 1240° C. or more, and cooled to obtain a clinker. (3) The clinker is mixed with at least one of sodium hydroxide and potassium hydroxide, and ground finely to produce a cement powder.
Claims10
A method of preparing an alkali-activated cement by stepwise calcination with sodium chloride, comprising:
- (1) mixing a sodium chloride, a silicate and a carbonate followed by grinding to obtain a raw material powder;
- (2) sequentially subjecting the raw material powder to a first calcination at 850-1050° C., a second calcination at 1240° C. or more and cooling to obtain a clinker;
- and
- (3) mixing the clinker with an alkali to produce the alkali-activated cement, wherein the alkali is sodium hydroxide, potassium hydroxide or a combination thereof;
- wherein a mixture of the silicate and the carbonate is adapted to produce a residue comprising SiO2, Al2O3, CaO, and MgO after oxidative calcination at 950±25° C.;
- a total weight of SiO2, Al2O3, CaO, and MgO accounts for 90.0% or more by weight of the residue;
- SiO2 accounts for 31.0-47.0% by weight of the residue;
- Al2O3 accounts for 12.4-18.0% by weight of the residue;
- CaO accounts for 21.3-46.3% by weight of the residue;
- and MgO accounts for 0-16.2% by weight of the residue;
- in the step (1), the sodium chloride is 8.0-20.0% by weight of the residue;
- and
- in the step (3), a weight of the alkali is calculated as follows:
- (a weight of NaOH+0.713×a weight of KOH)/a weight of the clinker=(0.5-3.0)%.
Dependencies are inferred from the claim text.