System and method for producing microcrystalline cellulose
AssigneeAndritz Inc.
InventorsKari VANHATALO, Hannu RÅMARK, Sonja PÄÄRNILÄ, Kari PELTONEN
Life of this patent
Estimating the term…
Abstract
A method for preparing microcrystalline cellulose (MCC) including: acid hydrolysis of a pulp mixture in at least one reactor to obtain a hydrolyzed process mixture, and mixing the hydrolyzed process mixture to form the MCC in the at least one reactor during the acid hydrolysis, wherein the mixing is performed with an energy dissipation around 1.0×106 W/m3 to 15.0×106 W/m3 and wherein a period of the mixing is in a range of 5 s to 180 s, and the MCC has an a to d ratio less than 6.0.
Claims22
-13. (canceled)
A method for preparing microcrystalline cellulose (MCC) comprising:
- acid hydrolysis of a pulp mixture in at least one reactor which generates a hydrolyzed process mixture, and
- mixing the hydrolyzed process mixture to form the MCC in the at least one reactor during the acid hydrolysis,
- wherein the mixing is performed with an energy dissipation in a range of 1.0×106 Watts per cubic meter (W/m3) to 15.0×106 W/m3,
- wherein a period of the mixing is in a range of 5 seconds (s) to 180 s, and
- wherein the MCC has a d-ratio no greater than 6.0.
A method comprising:
- treating pulp with acid hydrolysis in in at least one reactor to form a hydrolyzed pulp, and
- mixing the pulp during or after the treating to form a microcrystalline cellulose (MCC), wherein the mixing is performed with an energy dissipation in a range of 1.0×106 W/m3 to 15.0×106 watts per cubic meter (W/m3) and the mixing is performed in a range of 5 seconds(s) to 180 s,
- wherein the MCC has a d-ratio ((d90−d10)/d50) of no greater than 6.0,
- where d90 is a first micrometer size at which 90% of particles in the MCC are greater than, d10 is a second micrometer size at which 10% of the particles in the MCC are greater than, and d50 is a third micrometer size at which 50% of the particles in the MCC are greater than.
Dependencies are inferred from the claim text.