# US 2023/0143497 A1 · Device for closing the input opening in the sample chamber in an x-ray fluorescence spectrometer

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- Number: US 2023/0143497 A1
- Document ID: US20230143497A1
- Status: Published application
- Kind: A1
- Application number: 18/052,275
- Filed: 2022-11-03
- Published: 2023-05-11
- Earliest claimed: 2021-11-08
- Assignees: Bruker AXS GmbH
- Applicants: Bruker AXS GmbH
- Inventors: Wolfgang GEHRLEIN
- Web page: https://patentgrep.com/patent/US20230143497A1

## CPC

- G01N 23/2204: Specimen supports therefor; Sample conveying means therefore
- G01N 23/20025: Sample holders or supports therefor
- G01N 23/223: by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence
- G01N 2223/076: X-ray fluorescence
- G01N 2223/1016: X-ray
- G01N 2223/307: cuvettes-sample holders
- G01N 2223/321: manipulator for positioning a part
- G01N 2223/637: liquid
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

A closure device for the gas-tight closing of the input opening of a sample chamber of an x-ray analysis apparatus includes a slider having a closure plate and a carriage that is configured to be displaced in a lateral movement over the input opening on a linear guide arranged on a baseplate connected fixedly to the sample chamber. The closure plate is connected in an articulated manner to the carriage via deflecting elements that, upon butting against end stops connected rigidly to the baseplate, deflect the lateral movement of the carriage into a movement perpendicular thereto to press the closure plate over the input opening. A drive motor connected to the carriage via a drive means displaces the slider to provide the lateral movement on the linear guide.

## Claims

### Claim 1

A closure device for providing a gas-tight closing of an input opening of a sample chamber of an x-ray analysis apparatus, comprising:
a slider having a closure plate and a carriage that is configured to be displaced in a lateral movement over the input opening on a linear guide arranged on a baseplate connected fixedly to the sample chamber;
deflecting elements that connect the closure plate in an articulated manner to the carriage, the deflecting elements, upon butting against end stops connected rigidly to the baseplate, deflecting the lateral movement of the carriage into a movement perpendicular thereto to press the closure plate over the input opening; and
a drive motor that is connected to the carriage via a drive means and that displaces the slider to provide said lateral movement on the linear guide.

### Claim 2 (depends on 1)

The closure device as claimed in claim 1, wherein at least some of the deflecting elements are rotary levers.

### Claim 3 (depends on 2)

The closure device as claimed in claim 2, wherein the rotary levers comprise curved, rigid levers rotatably mounted on the carriage about a rigid shaft.

### Claim 4 (depends on 2)

The closure device as claimed in claim 2, wherein each rotary lever has a portion with an elongated hole that receives a pin connected rigidly to the closure plate.

### Claim 5 (depends on 2)

The closure device as claimed in claim 2, wherein the closure plate is rectangular, and wherein the deflecting elements comprise at least three of said rotary levers.

### Claim 6 (depends on 1)

The closure device as claimed in claim 1, wherein the linear guide comprises a guide rail arranged in or on the baseplate.

### Claim 7 (depends on 1)

The closure device as claimed in claim 1, further comprising a vertical guide device that guides the movement of the closure plate in said direction perpendicular to the lateral movement.

### Claim 8 (depends on 1)

The closure device as claimed in claim 1, further comprising spring spacer elements arranged between the closure plate and the carriage that hold the closure plate and the carriage apart at a predetermined distance.

### Claim 9 (depends on 1)

The closure device as claimed in claim 1, further comprising stop bolts attached to the closure plate that butt against said end stops when the carriage arrives at a first end of the baseplate.

### Claim 10 (depends on 1)

The closure device as claimed in claim 1, wherein the drive motor is an electric motor.

### Claim 11 (depends on 9)

The closure device as claimed in claim 9, wherein the drive motor is a stepping motor.

### Claim 12 (depends on 1)

The closure device as claimed in claim 1, wherein the drive means comprises at least one of a toothed belt drive, a drive chain, a push rod, a threaded spindle, a hydraulic slider, and a pneumatic cylinder.

### Claim 13 (depends on 12)

The closure device as claimed in claim 12, wherein the toothed belt drive and/or the drive chain run via a drive deflection roller and a belt pulley.

### Claim 14 (depends on 13)

The closure device as claimed in claim 13, wherein at least one of the drive deflection roller and the belt pulley are mounted resiliently, and tensioned with a predefined force, in the direction of the carriage relative to the baseplate, via a spring tensioning element.

### Claim 15 (depends on 1)

The closure device as claimed in claim 1, wherein at least one of the closure plate and the sample chamber has a sealing ring in a region around the input opening.

### Claim 16 (depends on 15)

The closure device as claimed in claim 15 wherein the sample chamber has a groove around the input opening that receives the sealing ring.

### Claim 17 (depends on 1)

An x-ray analysis apparatus comprising the closure device as claimed in claim 1.

### Claim 18

A method for providing a gas-tight closing of an input opening of a sample chamber of an x-ray analysis apparatus, the method comprising:
providing a slider having a closure plate and a carriage that is configured to be displaced in forward and return lateral movements over the input opening on a linear guide arranged on a baseplate connected fixedly to the sample chamber, the closure plate being connected in an articulated manner to the carriage with deflecting elements that butt against end stops connected rigidly to the baseplate when the slider is displaced in the forward lateral movement;
displacing the slider with a drive motor to provide said forward lateral movement on the linear guide;
when the deflecting elements butt against the end stops, transferring the forward lateral movement of the carriage into a movement perpendicular thereto with the deflecting elements to press the closure plate over the input opening; and
displacing the slider with the drive motor to provide the return lateral movement and reverse the closing of the input opening.
