Process for the preparation of dispersing agents in a solid form and their use in mineral binding compositions
AssigneeSika Technology AG
InventorsDenise MUTHS-KERN, Rasid SAHINAGIC, Christina HAMPEL, Jörg ZIMMERMANN, Nicole JAGIELSKI
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Abstract
A process for preparing powdered dispersants comprising at least 90% by weight of at least one copolymer CP of the polycarboxylate ether type. The powdered dispersants can be easily dispersed in water. The invention also relates to the use of such powdered dispersants in mineral binder compositions, in particular dry mortars, concrete or gypsum formulations.
Claims15
A process for producing a dispersant in solid form, wherein the dispersant comprises at least 90% by weight in each case based on the total weight of dispersant, of at least one copolymer CP, wherein the copolymers CP comprise the following constituents:
- (i) repeat units A of general structure (I),
- and
- (ii) repeat units B of general structure (II),
- where
- each Ru is independently hydrogen or a methyl group,
- each Rv is independently hydrogen or COOM, where M is independently H, an alkali metal, or an alkaline earth metal,
- m=0, 1, 2 or 3,
- p=0 or 1,
- each R1 is independently —[YO]n—R4, where Y is a C2 to C4 alkylene and R4 is H, C1 to C20 alkyl, cyclohexyl or alkylaryl, and n=2-350, and
- the repeat units A and B in the copolymer CP have a molar ratio
- A:B within a range from 10:90 to 90:10,
- wherein the process comprises the following steps:
- a) producing a mixture of at least one copolymer CP, at least one base, and water, wherein the molar ratio of base to copolymer CP is selected such that a degree of neutralization of at least 55%, results,
- b) optionally drying the neutralized aqueous preparation from step a), and
- c) optionally comminuting the material obtained in step b).
Dependencies are inferred from the claim text.