Hydroxyapatite powder and method for producing same
AssigneeChemische Fabrik Budenheim KG
InventorsErhard FISCHER, Stefan MALLMANN, Christian LITTERSCHEID
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Abstract
In order to provide a hydroxyapatite that can be used without reservation in the food industry, a hydroxyapatite powder is provided composed of primary particles. The median size of the primary particles from which the powder is made is >0.10 μm and the aspect ratio of the primary particles is <5. The specific surface area of the hydroxyapatite powder is ≤10 m2/g, and the bulk density is >550 g/l. Also disclosed is a method with which such a hydroxyapatite powder can be obtained.
Claims12
A hydroxyapatite powder composed of primary particles, wherein the median size of the primary particles is >0.10 and the aspect ratio of the primary particles is <5, wherein the specific surface area of the hydroxyapatite powder is ≤10 m2/g and the bulk density is >550 g/l.
A method for producing a hydroxyapatite powder, in which a reaction mixture is created in which milk of lime is reacted with phosphoric acid to form hydroxyapatite, wherein a method cycle comprising the following method steps is carried out:
- a) providing a suspension of hydroxyapatite starter particles in water,
- b) adding milk of lime and phosphoric acid to the suspension,
- c) reacting the milk of lime with the phosphoric acid in the suspension to form hydroxyapatite
- at a temperature in the range of >20° C. and <105° C. and
- at a pH in the range from 6.0 to 13.0,
- d) separating at least a portion of the hydroxyapatite particles out of the suspension,
- e) repeating method steps a) to d) at least once, wherein either the hydroxyapatite particles separated in method step d) or the hydroxyapatite particles remaining in the suspension in method step d) are used as the hydroxyapatite starter particles in method step a), and
- f) removing the hydroxyapatite particles which, in the dried state, have a median size of the primary particles of >0.1 μm from the method cycle.
Dependencies are inferred from the claim text.