# US 2022/0172923 A1 · X-Ray Detection Apparatus and Method > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 2022/0172923 A1 - Document ID: US20220172923A1 - Status: Published application - Kind: A1 - Application number: 17/534,865 - Filed: 2021-11-24 - Published: 2022-06-02 - Earliest claimed: 2020-11-27 - Assignees: JEOL Ltd. - Applicants: JEOL Ltd. - Inventors: Takanori Murano - Web page: https://patentgrep.com/patent/US20220172923A1 ## CPC - G01N 23/2252: Measuring emitted X-rays, e.g. electron probe microanalysis [EPMA] - H01J 37/28: with scanning beams {(H01J37/268, H01J37/292, H01J37/2955 take precedence)} - H01J 37/244: Detectors; Associated components or circuits therefor - G01N 2223/50: Detectors - H01J 2237/24425: Wavelength-dispersive spectrometer - H01J 2237/2446: Position sensitive detectors - H01J 2237/24585: Other variables, e.g. energy, mass, velocity, time, temperature - H01J 2237/2561: electron - H01J 2237/2801: Details - H01J 2237/2807: X-rays - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) - H01J: ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS (spark-gaps H01T; electric arc lamps H05B31/00; particle accelerators H05H) ## Abstract A mask member is provided at an entrance opening of a mirror unit. Of a first diffraction grating and a second diffraction grating, when the second diffraction grating is used, the mask member masks preceding mirrors. With this process, aberration caused by reflective X-ray is suppressed. When the first diffraction grating is used, the mask member does not function. Alternatively, the mask member and another mask member may be selectively used. ## Claims ### Claim 1 An X-ray detection apparatus comprising: a mirror unit comprising a reflective surface which applies light collection on an X-ray from an observation point on a sample; a spectroscopic device that applies spectral dispersion on the X-ray from the mirror unit, to thereby generate a dispersed X-ray which is spatially spread; an X-ray detector that detects the dispersed X-ray; and a mask member that is provided between the observation point and the mirror unit, and that partially covers the reflective surface, to thereby limit a reflective X-ray which is reflected by the reflective surface and reaches the spectroscopic device. ### Claim 2 (depends on 1) The X-ray detection apparatus according to claim 1, wherein the spectroscopic device comprises a first diffraction grating and a second diffraction grating which are selectively used, the first diffraction grating is placed at a first position when the first diffraction grating is used, the second diffraction grating is placed at a second position shifted from the first position in a first direction when the second diffraction grating is used, and the mask member limits the reflective X-ray reaching the second diffraction grating. ### Claim 3 (depends on 2) The X-ray detection apparatus according to claim 2, wherein the mirror unit comprises: a preceding subunit having two preceding mirrors which are distanced away from each other in a second direction orthogonal to the first direction; and a following subunit having two following mirrors which are distanced away from each other in the second direction, the reflective surface includes the two preceding mirrors, and the two following mirrors, and the mask member covers an entirety or a part of each of the preceding mirrors so that the mask member does not function when the first diffraction grating is used, and the reflective X-ray reaching the second diffraction grating is limited when the second diffraction grating is used. ### Claim 4 (depends on 3) The X-ray detection apparatus according to claim 3, wherein the preceding subunit has an entrance opening, and the mask member is provided at the entrance opening. ### Claim 5 (depends on 3) The X-ray detection apparatus according to claim 3, wherein the mask member comprises a pair of mask plates which are distanced away from each other in the second direction, and the mask plates cover the entirety or the part of each of the preceding mirrors when the second diffraction grating is used. ### Claim 6 (depends on 5) The X-ray detection apparatus according to claim 5, wherein the mask member comprises a connection plate which connects the pair of mask plates. ### Claim 7 (depends on 4) The X-ray detection apparatus according to claim 4, further comprising: a movement mechanism that places the mask member at the entrance opening when a priority-on-aberration-suppression mode is selected, and that retracts the mask member from the entrance opening when a priority-on-sensitivity mode is selected. ### Claim 8 (depends on 1) The X-ray detection apparatus according to claim 1, wherein the mask member is a first mask member which functions when the sample is observed, and the X-ray detection apparatus further comprises: a second mask member that is provided between the observation point and the spectroscopic device, that functions during calibration, and that allows a direct X-ray from the observation point to reach the spectroscopic device, and prevents the reflective X-ray from the reflective surface from reaching the spectroscopic device; and a mechanism that causes the first mask member and the second mask member to selectively function. ### Claim 9 A method of detecting an X-ray, the method comprising: applying, with a mirror unit, light collection on an X-ray from an observation point on a sample; applying, with a spectroscopic device, spectral dispersion on an X-ray from the mirror unit, to thereby generate a dispersed X-ray which is spatially spread; detecting the dispersed X-ray; and covering, with a mask member and at a location between the observation point and the mirror unit, a portion, of a reflective surface of the mirror unit, which causes an aberration, to thereby limit a reflective X-ray which is reflected by the reflective surface and reaches the spectroscopic device.