Process for production of needle coke
AssigneeIndian Oil Corporation Limited
InventorsPonoly Ramachandran PRADEEP, Shivam Ashok DIXIT, Prantik MONDAL, Jitumoni BRAHMA, * RAJESH, Terapalli Hari Venkata Devi PRASAD, Satyen Kumar DAS, Madhusudan SAU, Gurpreet Singh KAPUR, Sankara Sri Venkata RAMAKUMAR
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Abstract
High-quality graphite/needle grade coke is produced with reduced impurity levels and improved coefficient of thermal expansion using an integrated hydrotreatment, catalytic cracking and coking reaction sections, employing a combination of highly paraffinic hydrotreated VGO stream and aromatic CLO stream, which is thereafter processed in a delayed coking section.
Claims14
A process for production of graphite/needle grade coke with reduced impurity levels and improved coefficient of thermal expansion, wherein the process comprises:
- (a) routing a VGO feed to a riser reactor of a fluid catalytic cracking unit, wherein the VGO feed reacts with a hot catalyst supplied from a regenerator;
- (b) sending products of reaction from step (a) along with a catalyst to a stripper for separation of a hydrocarbon vapor product from the catalyst;
- (c) sending the hydrocarbon vapor product to a first fractionator column for separation into different products like off gases with naphtha, LCO, and HCO;
- (d) mixing a VGO stream with H2 and sending to a furnace for heating;
- (e) sending hot feeds from step (d) to a fixed bed reactor, wherein the hydrotreatment of a vacuum gas oil occurs and reaction products are sent to a high-pressure separator where lighter gases are removed and sent to a low-pressure separator;
- (f) sending remaining liquid to a second fractionator column for further separation of lighter products;
- (g) routing a hydrotreated VGO stream from the second fractionator column to a bottom section of the first fractionator column, wherein it is mixed with a CLO product fraction generated in the fluid catalytic cracking unit;
- (h) heat exchange between the hydrotreated VGO stream and the CLO product fraction occurring in the bottom section of the first fractionator column and forming a homogenous mixture;
- (i) sending the homogenous mixture through a parallel filtration assembly for separation of entrained catalyst fines present coming through the CLO product fraction;
- and
- (j) routing the homogenous mixture after catalyst removal to a third fractionator column of a delayed coking section.
An integrated system for production of graphite/needle grade coke, comprising:
- (a) a fluid catalytic cracking unit including:
- (i) a riser reactor;
- (ii) a regenerator;
- and
- (iii) a stripper for separation of vapor product;
- (b) a VGO hydrotreater including:
- (i) a furnace;
- (ii) a fixed bed reactor for hydrotreatment of vacuum gas oil;
- (iii) a high-pressure separator;
- and
- (iv) a second fractionator column for separation of lighter products;
- (c) a first fractionator column, wherein a hydrotreated VGO stream from the second fractionator column is mixed with a CLO product fraction generated in the fluid catalytic cracking unit;
- (d) a parallel filtration assembly for separation of entrained catalyst fines present coming through the CLO product fraction;
- and
- (e) a delayed coking section including:
- (i) a third fractionator column;
- (ii) a furnace;
- and
- (iii) coke drums.
Dependencies are inferred from the claim text.