Carbogenic nanoparticle-conducting polymer materials and inks for voc and moisture sensing, and methods of making and using the same
AssigneeNovatec, Inc.
InventorsLopamudra BHATTACHARJEE, Akshay SHARMA, Utpal MANNA, Ayush GOEL, Biplab PAL, Conrad BESSEMER
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Abstract
The present disclosure is directed to a carbogenic nanoparticle polymer inks including a conducting polymer, such as those made of CQD-PPy and/or R-GO-PPy, methods of making the inks, and moisture and VOC sensors made therefrom.
Claims32
A carbogenic nanoparticle-conducting polymer composite ink dispersed in water, wherein the carbogenic nanoparticle is reduced graphene oxide.
A carbogenic nanoparticle-conducting polymer composite ink dispersed in water selected from the group consisting of:
- R-GO-PPy composite ink, CQD-PANI composite ink, R-GO-PANI composite ink, CQD-PTH composite ink, R-GO-PTH composite ink, CQD-PA composite ink, R-GO-PA composite ink, CQD-PPP composite ink, R-GO-PPP composite ink, CQD-PPV composite ink, R-GO-PPV composite ink, CQD-PF composite ink, R-GO-PF composite ink, or a combination thereof.
A thin film coated PCB comprising:
- a thin film of a carbogenic nanoparticle-conducting polymer composite ink selected from the group consisting of:
- CQD-PPy composite ink, R-GO-PPy composite ink, CQD-PANI composite ink, R-GO-PANI composite ink, CQD-PTH composite ink, R-GO-PTH composite ink, CQD-PA composite ink, R-GO-PA composite ink, CQD-PPP composite ink, R-GO-PPP composite ink, CQD-PPV composite ink, R-GO-PPV composite ink, CQD-PF composite ink, R-GO-PF composite ink, or a combination thereof;
- and the PCB.
A method of making a thin film coated PCB comprising the steps of:
- treating the PCB under a UV lamp at about 260 nm to about 400 nm for about 15 minutes to about 60 minutes;
- and
- spin-coating the treated PCB with a carbogenic nanoparticle-conducting polymer composite ink comprising the steps of:
- i) horizontally positioning the treated PCB on a rotating disk of a spin-coating machine, under vacuum;
- ii) coating the substrate with a small amount of the composite ink;
- iii) rotating the coated PCB at one or more different speeds to obtain a first layer of composite ink on the PCB;
- and
- iv) optionally repeating steps ii and iii one to four times to obtain a double, triple, quadruple or quintuple layer of composite ink to make the thin film on the PCB.
A method of making a R-GO-conducting polymer composite ink comprising the steps of:
- a. Preparing graphene oxide (GO);
- b. Suspending the GO in water;
- c. Adding an iron (II) salt and a polymer having either a —COOH or a —SO3H group to the suspension to make an R-GO suspension;
- d. Acidifying the R-GO suspension;
- e. Adding a monomer of the conducting polymer to the acidified R-GO suspension to make a R-GO-conducting polymer composite suspension;
- f. Evaporating the composite suspension to reduce the volume to the composite ink.
Dependencies are inferred from the claim text.