Systems and methods for cannabis cbd extraction
AssigneePacific Import Manufacturing, Inc.
InventorMinyu Shi
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Abstract
Systems and methods for extracting a compound of interest from plant material, such as acannabidiol (CBD) from cannabis, are provided. Particularly, the disclosed systems and methods utilize a crude oil to separate water, fats, and proteins prior to preparation of a CBD distillate. The systems and methods are operable with conventional solvents containing between about 5 wt % and about 8 wt % water.
Claims20
A system for preparing a purified plant extract, comprising:
- a centrifugal separation unit, comprising at least one centrifugal separator, configured to receive plant material and a liquid solvent comprising ethanol, mix the plant material and the liquid solvent to form a slurry, and centrifuge the slurry in the centrifugal separator to separate the slurry into a solid residue and a raw extract, wherein the raw extract comprises at least one compound of interest and at least most of the liquid solvent;
- a filtration unit, comprising a filter assembly, configured to filter the raw extract to remove entrained solid plant material from the raw extract;
- a concentration unit, comprising an evaporator configured to receive the raw extract and heat the raw extract to remove at least most of the solvent therefrom by evaporation to thereby form a concentrated extract;
- a settling unit, comprising at least one settling vessel, configured to receive the concentrated extract and cause sedimentation of at least one impurity therefrom;
- a decarboxylation and degassing unit, comprising an atmosphere heating vessel and a vacuum heating vessel, wherein the atmosphere heating vessel is configured to receive the concentrated extract from the settling unit and heat the concentrated extract under approximately ambient or atmospheric pressure to decarboxylate at least a portion of the concentrated oil to form a decarboxylated oil, wherein the vacuum heating vessel is configured to receive the decarboxylated oil from the atmosphere heating vessel and heat the decarboxylated oil under sub-atmospheric pressure to form a winterized oil;
- and
- a short-path distillation unit, comprising at least one short-path distillation apparatus configured to receive the winterized oil from the decarboxylation and degassing unit and distill the winterized oil to form the purified plant extract.
A method for preparing a purified plant extract, comprising:
- (a) contacting plant material with a liquid solvent containing ethanol to form a slurry;
- (b) centrifuging the slurry to form a raw extract comprising at least one compound of interest and at least most of the liquid solvent;
- (c) filtering the raw extract to remove entrained solid plant material from the raw extract;
- (d) concentrating the raw extract by heating the raw extract to remove at least most of the solvent therefrom by evaporation to thereby form a concentrated extract;
- (e) precipitating a sediment comprising at least one impurity from the concentrated extract;
- (f) decarboxylating the concentrated extract by heating the concentrated extract under approximately ambient or atmospheric pressure to form a decarboxylated oil;
- (g) heating the decarboxylated oil under sub-atmospheric pressure to form a winterized oil;
- and
- (h) distilling the winterized oil by short-path distillation to form the purified plant extract.
A liquid composition, comprising at least about 70 wt % cannabinoids and terpenes and being substantially free of proteins and lipids.
Dependencies are inferred from the claim text.