# US 2021/0172089 A1 · Method for producing thread bundle derived from bagworm silk threads spun on the surface of a base material

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- Number: US 2021/0172089 A1
- Document ID: US20210172089A1
- Status: Published application
- Kind: A1
- Application number: 17/271,518
- Filed: 2019-08-27
- Published: 2021-06-10
- Earliest claimed: 2018-08-27
- Assignees: National Agriculture and Food Research Organization; Kowa Company, Ltd.
- Applicants: National Agriculture and Food Research Organization; Kowa Company, Ltd.
- Inventors: Taiyo YOSHIOKA; Tsunenori KAMEDA; Akimune ASANUMA; Norihiko FUKUOKA
- Web page: https://patentgrep.com/patent/US20210172089A1

## CPC

- D01C 3/02: De-gumming silk
- D01F 4/02: from fibroin
- D01F 4/00: Monocomponent artificial filaments or the like of proteins; Manufacture thereof
- D04H 1/4266: Natural fibres not provided for in group D04H1/425
- D01B 7/00: Obtaining silk fibres or filaments
- D01C: CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01F: CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D04H: MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL (weaving D03; knitting D04B; braiding D04C; net-making D04G; sewing D05B; tufting D05C; finishing non-woven fabrics D06); FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING {; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION}(non-woven fabrics having an intermediate or external layer of a different kind, e.g. of woven fabric, B32B)
- D01B: MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING (crude extraction of asbestos fibres from ores B03B; apparatus for retting D01C)

## Abstract

A bagworm silk thread spun on a base material was conventionally difficult to be collected, and thus, cannot be utilized. An object of the present invention is to develop and provide a method in which such a bagworm silk thread is peeled off from a base material with a weak force without being damaged and is collected as a thread bundle. Provided is a method for producing a thread bundle of a bagworm silk thread, including: applying, to a bagworm silk thread spun on the surface of a base material, a wetting liquid which presents a liquid form at least in the range of 20° C. or more and less than 30° C. and does not damage, denature, or dissolve the silk thread; and then separating the bagworm silk thread from the base material.

## Claims

### Claim 1

A method for producing a thread bundle of a bagworm silk thread, comprising:
wetting liquid applying process of applying a wetting liquid to the bagworm silk thread spun on the surface of a base material; and
separating the bagworm silk thread from the base material,
wherein the wetting liquid is in a liquid form at least in the range of 20° C. or more and less than 30° C. under the atmospheric pressure, and is a pure substance or a mixture that does not damage, denature, or dissolve a fibroin protein which is a fiber component of the bagworm silk thread.

### Claim 2 (depends on 1)

The method according to claim 1, further comprising a spinning process of placing a bagworm on the surface of the base material before the wetting liquid applying process and allowing the bagworm to spin the thread.

### Claim 3 (depends on 2)

The method according to claim 2, further comprising a bagworm collection process of collecting the bagworm together with a nest after the spinning process and before the wetting liquid applying process.

### Claim 4 (depends on 1)

The method according to claim 1, further comprising a washing process of washing the separated bagworm silk thread.

### Claim 5 (depends on 1)

The method according to claim 1, further comprising a degumming process of degumming the separated bagworm silk thread.

### Claim 6 (depends on 1)

The method according to claim 1, wherein the wetting liquid is a pure substance or a mixture that has a melting point of less than 20° C. and a boiling point of 30° C. or more and 300° C. or less.

### Claim 7 (depends on 1)

The method according to claim 1, wherein the wetting liquid is an aqueous solution or an organic solvent.

### Claim 8

A method for collecting a bagworm silk thread spun on the surface of a base material, comprising:
applying a wetting liquid to the bagworm silk thread spun on the surface of the base material; and
separating the bagworm silk thread from the base material,
wherein the wetting liquid is in a liquid form at least in the range of 20° C. or more and less than 30° C. under the atmospheric pressure, and is a pure substance or a mixture that does not damage, denature, or dissolve a fibroin protein which is a fiber component of the bagworm silk thread.

### Claim 9 (depends on 8)

The method according to claim 8, wherein the wetting liquid is an aqueous solution or an organic solvent.

### Claim 10 (depends on 1)

A bagworm silk thread(s) obtainable by the method according to claim 1.

### Claim 11 (depends on 1)

An unwoven fabric formed of a bagworm silk thread(s) obtainable by using the method for producing a thread bundle according to claim 1.

### Claim 12 (depends on 8)

A bagworm silk thread(s) obtainable by the method for collecting a bagworm silk thread according to claim 8.
