Advanced multi-functional asbestos free thermal insulating material and the process for preparation thereof
AssigneeCouncil of Scientific and Industrial Research
InventorsSarika VERMA, Sunil Kumar Sanghi, Mohammed Akram Khan, Sanjai Kumar Singh Rathore, Avanish Kumar Srivastava
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Abstract
The present invention relates to advanced multi-functional asbestos-free thermal insulating materials utilizing appropriate matrixes comprising nano thermal insulating precursor powder predominantly comprising calcium silicate and calcium magnesium silicate prepared from marble waste powder, rice husk and calcium hexametaphosphate; crushed silica fiberglass and a supporting matrix.
Claims10
A multi-functional asbestos-free thermal insulating material comprising:
- i. nano thermal insulating precursor powder comprising calcium silicate and calcium magnesium silicate prepared from 49.50-45.45% of marble waste powder, 49.50-45.45% of Rice husk and 1 to 9.1% of calcium hexametaphosphate;
- ii. crushed silica fiberglass;
- and
- iii. a supporting matrix;
- wherein the ratio of nano thermal insulating precursor powder, crushed silica fiberglass and the supporting matrix is in the range of 10:3:2.9 to 60:8:75.
A process for preparing a multi-functional asbestos free thermal insulating material comprising the steps of:
- a. dry grinding of 49.50-45.45% of marble waste powder;
- 49.50-45.45% of Rice husk and 1 to 9.1% of calcium hexametaphosphate in a ball mill or planetary mill for the period of 8 to 10 hours to obtain a grinded powder;
- b. mixing the grinded powder to aqueous solution of 50-80% potassium hydroxide to obtain a reaction mixture;
- c. irradiating the reaction mixture obtained in step (b) in microwave power of 200-350 watts for a duration of 10-15 minutes to obtain a precipitate;
- d. filtering the precipitate obtained in step (c) and drying it at 100° C.-110° C. to obtain solid powder of homogenized nano thermal insulating precursor;
- and
- e. treating the homogenized nano thermal insulating precursor of step (d) with supporting matrix selected from the group consisting of inorganic geopolymeric matrix, organo-chemical matrix, putty matrix, cement matrix and phosphatic matrix to obtain a multi-functional asbestos-free thermal insulating material.
Dependencies are inferred from the claim text.