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US 2020/0347518 A1Published application
Method of producing metal oxides with increased electrical conductivity
AssigneeShell Oil Company
InventorsMichael KANDIANIS, Oliver PLUEMPER
Life of this patent
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Abstract
A method for increasing the conductivity of a metal oxide with crystal structure belonging to the 4/m 32/m point group is provided. Single crystal oxides with crystal structure belonging to 4/m 32/m point group are contacted with nitrogen gas, with oxygen gas, with nitrogen gas, with oxygen gas, then with nitrogen gas to increase the conductivity of the metal oxide with crystal structure belonging to the 4/m 32/m point group.
Claims9
A method for increasing the conductivity of an oxide with crystal structure belonging to the 4/m 32/m point group comprising:
- (a) providing a single crystal oxide with crystal structure belonging to 4/m 32/m point group,
- (b) contacting the single crystal oxide with crystal structure belonging to 4/m 32/m point group with nitrogen gas at a temperature in the range of at least ambient temperature to at most 80° C. thereby providing a first nitrogen contacted metal oxide;
- (c) contacting the first nitrogen contacted metal oxide with oxygen gas at a temperature in the range of the range of at least ambient temperature to at most 80° C. thereby providing a first oxygen contacted metal oxide;
- (d) contacting the first oxygen contacted metal oxide with nitrogen gas at a temperature in the range of the range of at least ambient temperature to at most 80° C. thereby providing a second nitrogen contacted metal oxide;
- (e) contacting the second nitrogen contacted metal oxide with oxygen gas at a temperature in the range of at least 40° C. to at most 80° C. thereby providing a second oxygen contacted metal oxide;
- and
- (f) contacting the second oxygen contacted metal oxide with nitrogen gas at a temperature in the range of at least 40° C. to at most 80° C. thereby providing the increased conductivity crystalline metal oxide with a crystal structure belonging to 4/m 32/m point group oxide.
4 more elements
Dependencies are inferred from the claim text.