Method for producing methionine
AssigneeSumitomo Chemical Company, Limited
InventorsDaisuke YAMASHITA, Yoshiyuki KOIZUMI
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Abstract
An object of the present invention is to provide a method for producing methionine enabling efficient recovery and use of ammonia from a gas generated by concentrating a mother liquor. This production method comprises a recovery step of introducing a gas generated in a mother liquor concentration step into a gas washing tower in which water is recycled and bringing the gas into contact with the water to recover ammonia contained in the gas, and a ratio of flow of the water to flow of the gas introduced into the gas washing tower is 2 or more in terms of mass ratio. The water discharged from the gas washing tower is preferably cooled before introduction into the gas washing tower.
Claims2
A method for producing methionine comprising:
- a hydantoin step of reacting 3-methylmercaptopropionaldehyde and hydrocyanic acid, or a compound obtained by reacting 3-methylmercaptopropionaldehyde and hydrocyanic acid, with carbon dioxide and ammonia to obtain a liquid containing 5-(2-methylmercaptoethyl)hydantoin;
- a hydrolysis step of hydrolyzing the 5-(2-methylmercaptoethyl)hydantoin;
- a crystallization step of introducing carbon dioxide into a liquid containing a methionine salt obtained at the hydrolysis step to precipitate methionine;
- a separation step of separating a methionine slurry obtained in the crystallization step into solid and liquid;
- and
- a concentration step of concentrating a mother liquor obtained in the separation step,
- the method further comprising
- a recovery step of introducing a gas generated in the concentration step into a gas washing tower in which water is recycled and bringing the gas into contact with the water to recover ammonia contained in the gas, wherein
- a ratio of flow of the water to flow of the gas introduced into the gas washing tower is 2 or more in terms of mass ratio.
Dependencies are inferred from the claim text.