Synthesizing highly porous nanoparticles
AssigneeUnited States Government as represented by the Secretary of the Army
InventorDat Tien Tran
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Abstract
A system and method for synthesizing a nanoparticle material includes dissolving a metal nitrate in deionized water, adding a hydrogel precursor in the deionized water containing the dissolved metal nitrate to create an aqueous solution, heating the aqueous solution, cooling the aqueous solution to create a solid gel, and calcinating the solid gel to create a metal oxide nanoparticle material. The metal oxide nanoparticle material may include a zinc oxide-based nanoparticle material. The hydrogel precursor may include an agarose gel. The solid gel may be calcinated at approximately 600° C. The solid gel may be calcinated for approximately five hours in the presence of air. The aqueous solution may be heated to a boil. The aqueous solution may be heated at a temperature of ≤100° C.
Claims20
A method for synthesizing a nanoparticle material, the method comprising:
- dissolving a metal nitrate in deionized water;
- adding a hydrogel precursor in the deionized water containing the dissolved metal nitrate to create an aqueous solution;
- heating the aqueous solution;
- cooling the aqueous solution to create a solid gel;
- and
- calcinating the solid gel to create a metal oxide nanoparticle material.
A system for synthesizing a nanoparticle material, the system comprising:
- a first container comprising an aqueous solution containing a hydrogel precursor and deionized water comprising a dissolved metal nitrate;
- a first heat source to heat the aqueous solution;
- a second container to hold the aqueous solution during a cooling process to create a solid gel;
- and
- a second heat source to calcinate the solid gel to create a metal oxide nanoparticle material.
Dependencies are inferred from the claim text.