Back to results
US 2020/0048178 A1Published application
Method for producing polyfunctional acrylate
AssigneeOsaka Organic Chemical Industry Ltd.
InventorsKeisuke ITO, Shigeaki MATSUMOTO, Keita SHIGEMATSU
Life of this patent
Estimating the term…
Abstract
The present invention provides a production method of a multifunctional acrylate with a reduced tin content which includes adding an acid to a mixture containing an organotin compound and a multifunctional acrylate and distilling the mixture containing the acid.
Claims18
A method for producing a multifunctional acrylate with a reduced tin content comprising adding an acid to a mixture comprising an organotin compound and a multifunctional acrylate and distilling the mixture comprising the acid.
A method for producing a multifunctional acrylate comprising
- step 1 comprising a transesterification reaction of an acrylate and a polyhydric alcohol in the presence of an organotin compound to give a reaction mixture comprising the organotin compound and a multifunctional acrylate,
- step 2 comprising evaporating a compound having a boiling point lower than the organotin compound and the multifunctional acrylate from the reaction mixture to give a residue comprising the organotin compound and the multifunctional acrylate,
- step 3 comprising distilling the residue to give a distillate comprising the organotin compound and the multifunctional acrylate and a distillation residue comprising the organotin compound, and
- step 4 comprising adding an acid to the distillate and distilling the mixture comprising the acid to give a multifunctional acrylate with a reduced tin content.
1 more element
Dependencies are inferred from the claim text.