Black ziconia sintered body and preparation method therefor and use thereof
AssigneeShandong Sinocera Functional Material Co., Ltd.
InventorsAimin Yang, Xuekui Mo, Xibin Song
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Abstract
A black zirconia sintered body is obtained by processing and forming a powder for the black zirconia sintered body, and then sintering the same at a high temperature and normal pressure in the atmosphere. The powder for the black zirconia sintered body is prepared by a hydrothermal synthesis method using a soluble zirconium salt, a soluble yttrium salt and a color former as raw materials, wherein the molar ratio of the soluble zirconium salt, the soluble yttrium salt and the color former is 90-95:1-5:1-9. The black zirconia sintered body can be used in ceramic processes.
Claims13
A method of forming a powder for a black zirconia sintered body, the method comprising the following steps:
- S1, mixing a soluble zirconium salt and a soluble yttrium salt at a ratio and dissolving the zirconium salt and the yttrium salt in water to form a slurry, adding a coloring agent, and adjusting the pH of the slurry to 8 to 10 with ammonia water under stirring, wherein the molar ratio of the soluble zirconium salt, the soluble yttrium salt, and the coloring agent is 90 to 95:1 to 5:1 to 9;
- S2, subjecting the slurry to hydrothermal synthesis at 140 to 200° C. for 10 to 72 hours to form a resultant reaction solution;
- S3, washing the resultant reaction solution with water and drying to obtain a powder;
- S4, subjecting the powder to heat treatment at 800 to 1200° C. for 2 to 5 hours, and then grinding and dispersing the powder;
- and
- S5, granulating the dispersed particles to obtain the powder for a black zirconia sintered body.
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Dependencies are inferred from the claim text.