# US 2019/0170643 A1 · Apparatus and Method for Measuring Free Water in Hydrocarbon Fuels and Method of Calibrating the Apparatus > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 2019/0170643 A1 - Document ID: US20190170643A1 - Status: Published application - Kind: A1 - Application number: 15/830,042 - Filed: 2017-12-04 - Published: 2019-06-06 - Earliest claimed: 2017-12-04 - Assignees: Telectro-Mek, Inc. - Applicants: Telectro-Mek, Inc. - Inventors: James Edward Andrews, JR. - Web page: https://patentgrep.com/patent/US20190170643A1 ## CPC - G01N 21/643: {non-biological material} - G01N 21/645: {Specially adapted constructive features of fluorimeters} - G01N 21/77: by observing the effect on a chemical indicator - G01N 33/2847: {Water in oils} - G01N 2021/6439: {with indicators, stains, dyes, tags, labels, marks} - G01N 2021/7786: {Fluorescence} - G01N 2201/062: LED's - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) ## Abstract An apparatus and method of measuring free water, also known as undissolved water, in hydrocarbon fuel. A housing defines a chamber and is adapted to receive a fluorescein impregnated filter pad in the chamber between a UV light source and a light sensor. The filter pad is exposed to the fuel causing the free water to react with the fluorescein and is then placed within the chamber between the light source and sensor. The UV light strikes one side surface of the filter pad and excites the reacted fluorescein thereby causing light emitted from the UV light reacted fluorescein filter pad opposite side surface to strike the light sensor. An output from the light sensor is proportional to the fluorescein on the filter pad which reacted with free water and is used for providing an output value representative of the free water present in the hydrocarbon fuel. ## Claims ### Claim 1 A method of measuring free water in hydrocarbon fuel comprising the steps of: providing a housing comprising a UV light source and a light sensor and defining a chamber between the UV light source and the light sensor; exposing the hydrocarbon fuel to a fluorescein impregnated filter pad having opposing side surfaces thereby causing free water in the fuel to react with the fluorescein on the filter pad; placing the filter pad in the chamber between the UV light source and the light sensor thereby causing UV light from the UV light source to strike one side surface of the filter pad and excite the reacted fluorescein, and causing light emitted from the UV light reacted fluorescein filter pad opposite side surface to strike the light sensor; and, using an output from the light sensor to provide an output value representative of the free water present in the hydrocarbon fuel. ### Claim 2 (depends on 1) The method of claim 1 wherein only one side surface of the filter pad is impregnated with fluorescein and wherein, during the step of placing, the filter pad is placed in the chamber with its fluorescein impregnated side surface facing the light sensor. ### Claim 3 (depends on 1) The method of claim 1 wherein, during the step of placing, the filter pad side surfaces are located substantially perpendicular to a line extending between the UV light source and the light sensor. ### Claim 4 (depends on 1) The method of claim 1 further comprising providing a 300 nm to 500 nm light bandpass optical filter in the chamber between the UV light source and the filter pad. ### Claim 5 (depends on 1) The method of claim 1 further comprising providing a 500 nm to 650 nm light bandpass optical filter in the chamber between the filter pad and the light sensor. ### Claim 6 (depends on 1) The method of claim 1 further comprising providing a 400 nm light bandpass optical filter in the chamber between the UV light source and the filter pad. ### Claim 7 (depends on 1) The method of claim 1 further comprising providing a 550 nm light bandpass optical filter in the chamber between the filter pad and the light sensor. ### Claim 8 (depends on 1) The method of claim 1 wherein the UV light source is a 405 nm UV light mitting diode. ### Claim 9 (depends on 1) The method of claim 1 wherein the light sensor is a silicon photovoltaic diode detector. ### Claim 10 (depends on 1) The method of claim 1 wherein a plurality of light sensors are provided and, during the step of using, the outputs from each of the plurality of light sensors are averaged for providing the output value representative of the free water present in the hydrocarbon fuel. ### Claim 11 (depends on 1) The method of claim 1 wherein the light sensor comprises a camera. ### Claim 12 (depends on 1) The method of claim 1 wherein the light sensor comprises a camera and wherein, during the step of using, a digital image output from the camera is divided into pixel areas, each of the pixel areas are assigned a weighted value proportional to the light received at that pixel area and the weighted values are then averaged for providing the output value representative of the free water present in the hydrocarbon fuel. ### Claim 13 (depends on 1) The method of claim 1 wherein a receiving slot is provided through the housing leading to the chamber and wherein, after the step of exposing, the filter pad is secured on a tray and is placed in the chamber by sliding the tray through the receiving slot into the chamber and between the UV light source and the light sensor. ### Claim 14 (depends on 13) The method of claim 13 wherein the tray comprises a pair of arms and the arms comprise aligned openings and, during the step of securing the filter pad on the tray, the filter pad side surfaces are aligned with the openings of the arms and a perimeter edge of the filter pad is clamped between the arms. ### Claim 15 (depends on 14) The method of claim 14 wherein an annular recess seat is provided around one arm opening and an annular protruding boss is provided around the other arm opening and wherein, during the step clamping, the filter pad perimeter edge is placed within the annular recess and the annular boss is received within the annular recess thereby clamping the perimeter edge between the annular recess and the annular boss. ### Claim 16 (depends on 1, 13) The method of claim 13 wherein, after the step of sliding the tray through the receiving slot, the tray effectively closes the receiving slot and prevents ambient light from entering the chamber. 17, The method of claim 1 wherein only one side surface of the filter pad is impregnated with fluorescein and wherein, during the step of placing, the filter pad is placed in the chamber with its fluorescein impregnated side facing the light sensor and wherein, during the step of placing, the filter pad is placed substantially perpendicular to a line extending between the UV light source and the light sensor. ### Claim 18 (depends on 17) The method of claim 17 further comprising providing a 300 nm to 500 nm light bandpass optical filter in the chamber between the UV light source and the filter pad, and providing a 500 nm to 650 nm light bandpass optical filter in the chamber between the filter pad and the light sensor. ### Claim 19 (depends on 18) The method of claim 18 wherein a receiving slot is provided through the housing leading to the chamber and wherein, after the step of exposing, the filter pad is secured on a tray and is placed in the chamber by sliding the tray through the receiving slot into the chamber and between the UV light source and the light sensor. ### Claim 20 (depends on 19) The method of claim 19 wherein, after the step of sliding the tray through the receiving slot, the tray effectively closes the receiving slot and prevents ambient light from entering the chamber.