Method for producing separation membrane using mfi-type zeolite (silicalite)
AssigneeHitachi Zosen Corporation
InventorsKazuhiro YANO, Masaya ITAKURA, Kentaro SHINOYA, Satoshi IMASAKA
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AssigneeHitachi Zosen Corporation
InventorsKazuhiro YANO, Masaya ITAKURA, Kentaro SHINOYA, Satoshi IMASAKA
Estimating the term…
Provided is a method for producing a separation membrane including a silicalite membrane without using NaOH or the like that causes an increase in cost with respect to equipment, facilities, and process time. The method for producing a separation membrane is a method for producing a separation membrane including a porous support and a silicalite membrane that is formed on the support and has an MFI-type zeolite crystal structure, and is characterized in that the method includes a step of producing a seed crystal, a step of attaching the seed crystal onto the porous support, a step of producing a membrane synthesis raw material composition containing SiO2, an organic template, and H2O, and a step of immersing the porous support having the seed crystal attached thereto in the membrane synthesis raw material composition and performing hydrothermal synthesis, and the composition ratio of the membrane synthesis raw material composition is as follows: SiO2:organic template:H2O=1:(0.05 to 0.15):(50 to 120).
1-6. (canceled)
A method for producing a separation membrane which includes a porous support and a silicalite membrane that is formed on the support and has an MFI-type zeolite crystal structure, characterized in that the method comprises:
The method for producing a separation membrane according to 7, characterized in that the average particle diameter dseed of the seed crystal and the surface layer portion average pore diameter dsupport of the porous support have a relationship represented by the following formula (1):
Dependencies are inferred from the claim text.