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US 2019/0055364 A1Published application
Process for preparing a silicone elastomer and personal care composition containing the elastomer
AssigneeConopco, Inc., d/b/a UNILEVER
InventorsAdam John LIMER, Anjing LOU, Brian John DOBKOWSKI, Wei ZHAO, Wenhui SONG
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Abstract
A method for preparing silicone elastomers containing hydrophobic skin actives with excellent characteristics is described. The elastomer shows enhanced efficacy with respect to the skin actives compared to skin care compositions formulated with individual elastomer and active(s) components. Skin care compositions containing the inventive silicone elastomers and methods of skin treatment are also described.
Claims14
A method for making a silicone elastomer with entrapped hydrophobic active, comprising the steps of:
- 1. combining, in no particular order:
- (i) 0.05 to 8% by weight of a hydride functionalized silicone elastomer precursor;
- (ii) 2 to 60% by weight of a vinyl functionalized silicone elastomer precursor;
- (iii) 0.5 to 97% by weight of a solvent comprising polydimethylsiloxane or caprylyl trimethicone;
- (iv) 0.25 to 65% by weight hydrophobic active;
- and
- (v) catalyst at an amount effective to catalyze polymerization of the hydride and vinyl functionalized elastomer precursors;
- and
- 2. recovering silicone elastomer with entrapped hydrophobic active, wherein:
- (i) the hydrophobic active is soluble in the solvent;
- and
- (ii) at least 20% of total solvent used to make the silicone elastomer is provided before polymerization is initiated wherein any remainder of solvent used is provided gradually within 5 to 30 minutes in further swelling of elastomer when polymerization of the hydride is 90 to 99% complete and the silicone elastomer with entrapped hydrophobic active has a viscosity from 50 to 3000 cps and a G′ storage modulus from 700 to 10,000PA
- (iii) the hydrophobic active is a sunscreen, oil soluble vitamin, hydroxyacid, or resorcinol.
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Dependencies are inferred from the claim text.