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US 2018/0297852 A1Published application
Fluidized bed reactor and process for producing polycrystalline silicon granules
AssigneeWacker Chemie AG
InventorsSimon PEDRON, Bernhard BAUMANN
Life of this patent
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Abstract
Campaigns for the production of polycrystalline silicon granules in a fluidized bed process are lengthened by employing an inner reaction tube within the fluidized bed reactor which has a low ash content, preferably a coefficient of thermal expansion similar to that of silicon carbide, and has a silicon carbide coating layer consisting of at least 99.995 wt. % of silicon carbide with a thickness of from 5 μm to 700 μm.
Claims13
-11. (canceled)
A fluidized-bed reactor for producing granular polycrystalline silicon, comprising:
- a reactor vessel, and a reactor tube and a reactor bottom within the reactor vessel, wherein the reactor tube comprises a main element with a surface coating, and an intermediate jacket is present between an outer wall of the reactor tube and an inner wall of the reactor vessel, and further comprising a heating device, at least one fluidizing gas nozzle for introduction of a fluidizing gas and at least one reaction gas nozzle for introduction of reaction gas, a silicon seed particle feed for introducing silicon seed particles, an offtake conduit for granular polycrystalline silicon product and a reactor offgas discharge, wherein the main element of the reactor tube comprises a base material having an ash content of <2000 ppmw and the surface coating is a CVD coating which has a layer thickness of from 5 μm to 700 μm and comprises at least 99.995 % by weight of silicon carbide.
Dependencies are inferred from the claim text.