Hydrochloric acid purification process
AssigneeArkema France
InventorsBertrand COLLIER, Dominique DEUR-BERT, Joaquin LACAMBRA, Anne PIGAMO
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Abstract
The invention relates to a process for the treatment of a gas stream comprising hydrochloric acid, hydrofluoric acid and fluorinated/oxygenated compounds, in which the gas stream is successively subjected to: a stage of catalytic hydrolysis; a stage of washing with an acid solution; a stage of adsorption of impurities by active charcoal; a stage of adiabatic or isothermal absorption of the hydrochloric acid in an aqueous solution, making it possible to collect hydrochloric acid solution.
Claims21
1-20. (canceled)
A process for treating a gas stream comprising hydrochloric acid, hydrofluoric acid and fluorinated/oxygenated compounds, comprising successively subjecting the gas stream to the following stages:
- a stage of catalytic hydrolysis;
- a stage of washing with an acid solution;
- a stage of adsorption of impurities by active charcoal;
- and
- a stage of adiabatic or isothermal absorption of the hydrochloric acid in an aqueous solution, thereby making it possible to collect hydrochloric acid solution.
A plant for the treatment of a gas stream comprising hydrochloric acid, hydrofluoric acid and fluorinated/oxygenated compounds, comprising:
- a pipe for feeding a gas stream comprising hydrochloric acid, hydrofluoric acid and fluorinated/oxygenated compounds to a catalytic hydrolysis unit;
- a washing unit, fed, on the one hand, by a pipe for collecting the hydrolyzed gas stream resulting from the catalytic hydrolysis unit and, on the other hand, by a pipe for introducing an acid solution;
- a unit for adsorption of impurities comprising a bed of active charcoal, which unit is fed by a pipe for collecting the washed gas stream resulting from the washing unit;
- a unit for adiabatic or isothermal absorption, fed, on the one hand, by a pipe for collecting the purified stream resulting from the adsorption unit and, on the other hand, by a pipe for introducing an aqueous solution;
- and
- a pipe for collecting a hydrochloric acid solution at the outlet of the adiabatic absorption unit.
Dependencies are inferred from the claim text.