# US 2016/0258741 A1 · Using tunable lasers in the design, manufacture, and implementation of integrated optical elements

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- Number: US 2016/0258741 A1
- Document ID: US20160258741A1
- Status: Published application
- Kind: A1
- Application number: 14/408,354
- Filed: 2013-12-19
- Published: 2016-09-08
- Earliest claimed: 2013-12-19
- Assignees: Halliburton Energy Services, Inc.
- Applicants: Halliburton Energy Services, Inc.
- Inventors: David L. Perkins
- Web page: https://patentgrep.com/patent/US20160258741A1

## CPC

- G01B 11/0675: {using interferometry}
- G01N 21/211: {Ellipsometry (optical thickness measurement G01B11/06)}
- G01N 21/39: using tunable lasers
- G01N 21/8422: {Investigating thin films, e.g. matrix isolation method}
- H01S 3/1083: {using parametric generation}
- H01S 3/13: Stabilisation of laser output parameters, e.g. frequency or amplitude
- G01J 4/04: Polarimeters using electric detection means (G01J4/02 takes precedence)
- G01B: MEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- H01S: DEVICES USING THE PROCESS OF LIGHT AMPLIFICATION BY STIMULATED EMISSION OF RADIATION [LASER] TO AMPLIFY OR GENERATE LIGHT; DEVICES USING STIMULATED EMISSION OF ELECTROMAGNETIC RADIATION IN WAVE RANGES OTHER THAN OPTICAL
- G01J: MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY (light sources F21, H01J, H01K, H05B; investigating properties of materials by optical means G01N)

## Abstract

Disclosed are systems and methods that use a tunable laser during optical thin-film fabrication. One disclosed system includes a tunable laser capable of generating electromagnetic radiation, one or more thin-film devices arranged to receive the electromagnetic radiation, each thin-film device including one or more optical layers deposited on a corresponding substrate and configured to generate optically interacted radiation upon receiving the electromagnetic radiation, and an optical transducer arranged to receive the optically interacted radiation from each of the one or more thin-film devices and configured to generate output signals corresponding to the optically interacted radiation received from each of the one or more thin-film devices.

## Claims

### Claim 1

A system, comprising:
a tunable laser capable of generating electromagnetic radiation;
one or more thin-film devices arranged to receive the electromagnetic radiation, each thin-film device including one or more optical layers deposited on a corresponding substrate and configured to generate optically interacted radiation upon receiving the electromagnetic radiation; and
an optical transducer arranged to receive the optically interacted radiation from each of the one or more thin-film devices and configured to generate output signals corresponding to the optically interacted radiation received from each of the one or more thin-film devices.

### Claim 2 (depends on 1)

The system of claim 1, further comprising a polarizer configured to receive and polarize the electromagnetic radiation.

### Claim 3 (depends on 1)

The system of claim 1, wherein the one or more thin-film devices are optical thin-films.

### Claim 4 (depends on 3)

The system of claim 3, wherein the optical thin-films are integrated computational elements.

### Claim 5 (depends on 1)

The system of claim 1, wherein the tunable laser further comprises an optical parametric oscillator.

### Claim 6 (depends on 1)

The system of claim 1, further comprising an intensity filter arranged in an optical path between the tunable laser and the optical transducer.

### Claim 7 (depends on 1)

The system of claim 1, wherein the one or more thin-film devices are arranged on an assembly.

### Claim 8 (depends on 7)

The system of claim 7, wherein the assembly is capable of moving relative to the source and detector in at least one direction in order to expose the one or more thin-films devices to the electromagnetic radiation.

### Claim 9 (depends on 1)

The system of claim 1, wherein the one or more thin-film devices are arranged within a fabrication housing.

### Claim 10 (depends on 9)

The system of claim 9, wherein the fabrication housing further includes one or more sample windows configured to allow the electromagnetic radiation and optically interacted radiation to pass therethrough.

### Claim 11 (depends on 1)

The system of claim 1, further comprising a signal processor configured to receive the output signals and determine one or more parameters corresponding to the one or more thin-film devices.

### Claim 12 (depends on 11)

The system of claim 11, wherein the signal processor includes a machine-readable storage medium that includes at least one model or data set capable of correlating amplitude and phase data of optically interacted radiation to refractive indices, and wherein the signal processor is configured to determine the one or more parameters by comparing the output signals with the at least one model or data set.

### Claim 13 (depends on 11)

The system of claim 11, wherein the signal processor is further configured to output a resulting output signal indicative of the one or more parameters of the one or more thin-film devices.

### Claim 14

A method, comprising:
generating electromagnetic radiation from a tunable laser;
receiving the electromagnetic radiation with one or more thin-film devices, each of the one or more thin-film devices including one or more optical layers deposited on a corresponding substrate;
generating optically interacted radiation from each of the one or more thin-film devices upon receiving the electromagnetic radiation;
receiving the optically interacted radiation with an optical transducer; and
generating output signals with the optical transducer corresponding to the optically interacted radiation received from each of the one or more thin-film devices.

### Claim 15 (depends on 14)

The method of claim 14, further comprising receiving and polarizing the electromagnetic radiation with a polarizer.

### Claim 16 (depends on 14)

The method of claim 14, further comprising tuning the electromagnetic radiation with an optical parametric oscillator associated with the tunable laser.

### Claim 17 (depends on 14)

The method of claim 14, further comprising reducing an intensity of the electromagnetic radiation or the optically interacted radiation with an intensity filter arranged in an optical path between the tunable laser and the optical transducer.

### Claim 18 (depends on 14)

The method of claim 14, further comprising:
receiving the output signals with a signal processor communicably coupled to the optical transducer, the signal processor comprising a machine-readable storage medium including at least one model or data set correlating amplitude and phase data of optically interacted radiation to refractive indices;
determining one or more parameters of each thin-film device with the signal processor based on the output signals and the at least one model or data set correlating amplitude and phase data of optically interacted radiation to refractive indices; and
generating resulting output signals from the signal processor corresponding to the one or more parameters.

### Claim 19 (depends on 18)

The method of claim 18, wherein determining the one or more parameters of each thin-film device comprises determining an amplitude and a phase of the optically interacted radiation.

### Claim 20 (depends on 18)

The method of claim 18, wherein determining the one or more parameters of each thin-film device comprises determining a refractive index of the one or more optical layers by comparing the output signals to the at least one model or data set of the machine-readable storage medium.

### Claim 21 (depends on 18)

The method of claim 18, wherein determining the one or more parameters of each thin-film device comprises determining a thickness of the one or more optical layers of the one or more thin-film devices.

### Claim 22 (depends on 18)

The method of claim 18, further comprising:
scanning a spectrum of wavelengths with the tunable laser and thereby altering the output signals;
receiving the altered output signals correlating to the scanned spectrum with the signal processor; and
storing at least a portion of the altered output signals as one of the one or more models or data sets.

### Claim 23

A system, comprising:
a tunable laser capable of generating electromagnetic radiation;
a fluid within a flow path and configured to optically interact with the electromagnetic radiation, thereby generating optically interacted radiation;
one or more thin-film devices arranged to receive the optically interacted radiation, each thin-film device including one or more optical layers deposited on a corresponding substrate and configured to generate modified electromagnetic radiation upon optically interacting with the optically interacted radiation; and
an optical transducer arranged to receive the modified electromagnetic radiation from each of the one or more thin-film devices and configured to generate corresponding output signals therefrom.

### Claim 24

A system, comprising:
a tunable laser capable of generating electromagnetic radiation;
a fluid within a flow path and configured to optically interact with the electromagnetic radiation, thereby generating optically interacted radiation;
an optical element configured to interact with the electromagnetic radiation and thereby generate reduced intensity electromagnetic radiation;
an optical transducer arranged to receive at the optically interacted radiation and generate a corresponding first output signal, and further configured to receive the reduced intensity electromagnetic radiation and generate a corresponding second output signal; and
a signal processor configured to receive the first and second output signals from the optical transducer and determine a characteristic of the fluid based on the first and second output signals.

### Claim 25 (depends on 24)

The system of claim 24, wherein the optical element is an interference filter.
