Process for producing a blank, and a blank
AssigneeDENTSPLY International Inc.
InventorsStefan FECHER, Heiner HÖRHOLD, Udo SCHUSSER, Markus VOLLMANN, Martin KUTZNER
Life of this patent
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Abstract
The invention relates to a blank for producing a dental moulded part such as an inlay, onlay, crown or bridge, and to a method for producing the blank. To be able to machine a dental moulded part, in particular one having thin wall thicknesses, from the blank without difficulty, the blank is designed to consist of a glass ceramic having a density of between 30 and 60% of theoretical density, and of glass-ceramic powder particles with a particle size distribution d90≦80 μm, lithium silicate crystals being present in an amount of 10 to 90% by volume.
Claims27
A blank for producing a dental molded part, the blank comprising:
- lithium silicate crystals;
- glass ceramics with a density between 30% and 60% of a theoretical density of a fully-sintered blank;
- and
- glass-ceramic powder particles with a grain size distribution d90≦80 μm;
- wherein a fraction of lithium silicate crystals is between 10% by volume and 90% by volume.
A method for producing a dental molded part, the method comprising the steps of:
- producing a molten mass with a composition (in % by weight):
- SiO2 46.0-72.0;
- Li2O 10.0-25.0;
- ZrO2 6.5-14.0;
- P2O5 1.0-10.0;
- Al2O3 0.1-8.0;
- K2O 0.1-5.0;
- CeO2 0.1-4.0;
- B2O3 0.0-4.0;
- Na2O 0.0-4.0;
- Tb4O7 0.0-2.5;
- and
- 0.0 to 4.0 of at least one additive,
- producing a glass frit by atomizing the molten mass and quenching the molten mass in a medium,
- generating glass powder particles from the glass frit with a grain size distribution d90<80 μm,
- crystallizing lithium silicate crystals with a volume fraction between 10% and 90% by a first thermal treatment of either the glass frit or the glass powder particles in a first temperature range at a temperature T1 with 500° C.≦T1≦750° C. for a duration t1 with 5 min≦t1≦120 min, whereby, glass-ceramic powder particles with a grain size distribution d90≦80 μm are produced from a heat-treated glass frit,
- pressing the glass-ceramic powder particles to form a blank,
- machining the blank by milling to produce a pre-form part corresponding to the dental molded part, taking into consideration the shrinkage characteristics of the blank, and
- sintering the pre-form part at a temperature T2 with 800° C.≦T2≦1050° C. for a duration t2 with 5 min≦t2≦60 min.
Dependencies are inferred from the claim text.