Method for removing volatile components from elastomer-containing media and degassing devices therefor
AssigneeLanxess International SA
InventorsHanns-Ingolf PAUL, Joerg KIRCHHOFF, Udo WIESNER, Luc TIMMERMANS, Nicolai DIELTIENS
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Abstract
The invention relates to a method for degassing elastomer-containing media, such as elastomer solutions and dispersions in particular, and degassing devices (1) for carrying out said method.
Claims27
A treatment and degassing device comprising at least one extruder, the extruder comprising:
- a housing and n housing bores Bn with corresponding bore diameters Dn, where n is a whole number from 2 to 16, and wherein the housing bores intersect and are parallel to one another;
- n shafts Wn, configured to rotate 360° in the same direction and each of which is arranged concentrically in one of the housing bores Bn, each of which has a rotational axis An and each of which is provided with at least one treatment element whose cross-sectional profile, in the peripheral direction, has:
- m relative maxima Rmmax n in respect of the radial extension of the cross-section profile of the treatment element to the rotating axis An of the shaft Wn, where m is a whole number from 1 to 16, wherein, in addition, at least one relative maximum Rmmax n is an absolute maximum of the radial extension Rmmax n in respect of the radial extension of the cross-sectional profile of the treatment element to the rotational axis An of the shaft Wn, wherein:
- Rmax nn<=(Dn/2),
- at least one feed zone,
- one or more degassing zones, each comprising at least one degassing vent, configured for discharging volatile components from a medium containing elastomers from the extruder,
- at least one discharge zone,
- wherein the treatment elements comprise screw elements SE, wherein:
- a clearance ASE between the profiles of the screw elements of two shafts, each of which is arranged concentrically in adjacent housing bores Bn and Bn+1,
- i) from 0.001 to 0.2 AD, wherein AD is the clearance between the rotational axes of the two adjacent shafts,
- ii) and has at least one absolute minimum AminSE and one absolute maximum AmaxSE, wherein AmaxSE is ≦1.5 AminSE.
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The method in accordance with claim, wherein the medium containing elastomers (EM) comprises styrene-butadiene, natural rubbers (NR), butadiene rubbers (BR), isoprene rubbers (IR), ethylene-propylene-diene rubbers, ethylene-propylene rubbers, nitrile rubbers, hydrogenated nitrile rubbers (HNBR), butyl rubbers, halo-butyl rubbers, or ionomers produced from halobutyl rubbers by conversion using amines or phosphines, chloroprene rubbers (CR), ethylene vinyl acetate rubbers (EVA and EVM), polyurethane rubbers, gutta-percha, fluoro rubbers, silicone rubbers, sulfide rubbers, chloride-sulfonyl polyethylene rubbers, as well as any mixtures of the abovementioned elastomers.
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Dependencies are inferred from the claim text.