Apparatus and method for measuring hydrogen peroxide in water
AssigneeSpi Technology Ltd.
InventorsJim SHUBAT, Gerben OP DEN BUIJS, Ludo FEYEN
Life of this patent
Estimating the term…
Abstract
An apparatus and method for measuring hydrogen peroxide concentration in water to an accuracy of 0.1 ppm comprises a colorimetric assay method to determine hydrogen peroxide concentration. The assay is monitored spectophotometrically at a desired wavelength. Each sample is corrected relative to a control sample and hydrogen peroxide concentration determined with respect to a standard curve.
Claims15
An apparatus for measuring hydrogen peroxide in water using a colorimetric assay method comprising:
- a. a measurement cell for containing a water sample;
- b. a light transmitter configured to emit light at a selected wavelength at the measurement cell;
- c. a photodiode receiver configured to receive light passing through the measurement cell;
- d. a reagent in a reagent vial, consisting of:
- a reagent compound configured to react with hydrogen peroxide to form a reaction product, the reaction product adapted to absorb light at the selected wavelength proportional to the amount of hydrogen peroxide in the water sample,
- a surfactant, and
- a solvent;
- and
- e. a first network of pipes connecting the source water to a buffer jar, the buffer jar to a supply valve, the supply valve to the measurement cell, and a second network of pipes connecting the reagent vial to a reagent valve, the reagent valve to the measurement cell, and the measurement cell to a drain valve;
- f. a control unit;
- wherein the control unit is configured to cause a first colorimetric measurement of a first water sample free of reagent and a second colorimetric measurement of a second water sample mixed with reagent, then determines the difference between the first and second measurements and compares the difference against a pre-determined standard curve of diluted hydrogen peroxide to determine and report the concentration of hydrogen peroxide in the water sample, accurate to 0.1 mg/L.
A method of for measuring hydrogen peroxide levels in water using a colorimetric assay method comprising:
- a. transferring a first water sample to a measuring cell;
- b. determining a first absorbance measurement of light at a selected wavelength as a null measurement;
- c. removing the first sample from the measurement cell;
- d. transferring an aliquot of a reagent consisting of a reagent compound configured to react with hydrogen peroxide, reacts to form a reaction product, the reaction product adapted to absorb light at the selected wavelength proportional to the amount of hydrogen peroxide in the water sample to the measurement cell;
- e. filling the measurement cell with a second water sample;
- f. determining a second absorbance measurement of light at the selected wavelength as a test measurement;
- g. emptying the measurement cell and rinsing with sample water;
- and
- h. a control unit adapted to determine the difference between the first and second measurements and compare the difference against a pre-determined standard curve of diluted hydrogen peroxide to determine and report the concentration of hydrogen peroxide in the water sample to an accuracy of 0.1 mg/L.
Dependencies are inferred from the claim text.