# US 2014/0290802 A1 · Surface treatment method and coating method for steel material, and method for producing machine component

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- Number: US 2014/0290802 A1
- Document ID: US20140290802A1
- Status: Published application
- Kind: A1
- Application number: 14/350,724
- Filed: 2012-09-12
- Published: 2014-10-02
- Earliest claimed: 2011-10-25
- Assignees: Komatsu Ltd.; Nippon Kazai Co., Ltd.; Cotec Corporation
- Inventors: Haruji Morita; Tsuneo Tate; Akira Shiozawa
- Web page: https://patentgrep.com/patent/US20140290802A1

## CPC

- C23C 8/42: only one element being applied
- C23C 8/80: After-treatment
- C23C 22/08: Orthophosphates
- C23C 22/47: containing also phosphates
- C23C 22/83: Chemical after-treatment
- C23C: COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL (making metal-coated products by extrusion B21C23/22; covering with metal by connecting pre-existing layers to articles, see the relevant places, e.g. B21D39/00, B23K; metallising of glass C03C; metallising mortars, concrete, artificial stone, ceramics or natural stone C04B41/00; enamelling of, or applying a vitreous layer to, metals C23D; treating metal surfaces or coating of metals by electrolysis or electrophoresis C25D; single-crystal film growth C30B; by metallising textiles D06M11/83; decorating textiles by locally metallising D06Q1/04)

## Abstract

This surface treatment method comprises a rustproofing step, a rinsing step, and a cleaning step. In the rustproofing step, a rustproofing liquid containing orthophosphoric acid and an organic acid is used to perform a rustproofing treatment on the surface of a steel material. In the rinsing step, a treatment liquid containing an oxo acid salt of a transition metal is used to perform a rinsing treatment on the surface of the steel material. In the cleaning step, the surface of the steel material that has undergone the rinsing step is subjected to a cleaning treatment.

## Claims

### Claim 1

A surface treatment method for a steel material, comprising:
a rustproofing step of using a rustproofing liquid containing orthophosphoric acid and an organic acid to perform a rustproofing treatment on the a surface of a steel material;
a rinsing step of using a treatment liquid containing an oxo acid salt of a transition metal to perform a rinsing treatment on the surface of the steel material; and
a cleaning step of subjecting the surface of the steel material that has undergone the rinsing step to a cleaning treatment.

### Claim 2 (depends on 1)

The surface treatment method for a steel material according to claim 1,
further comprising a degreasing step of using a degreasing liquid to remove oil and grease from the surface of the steel material.

### Claim 3 (depends on 2)

The surface treatment method for a steel material according to claim 2,
further comprising a first water washing step of washing the surface of the steel material that has undergone the degreasing step.

### Claim 4 (depends on 1)

The surface treatment method for a steel material according to claim 1,
further comprising a second water washing step of using a treatment liquid containing orthophosphoric acid and an organic acid to wash the surface of the steel material that has undergone the rustproofing step.

### Claim 5 (depends on 1)

The surface treatment method for a steel material according to claim 1,
further comprising a spray step of spraying water on the surface of the steel material that has undergone the cleaning step.

### Claim 6 (depends on 1)

The surface treatment method for a steel material according to claim 1,
wherein a treatment liquid containing sodium dihydrogen phosphate dihydrate, a fluorine-based surfactant, and special modified ionized water is used in the rustproofing step and the second water washing step.

### Claim 7 (depends on 1)

The surface treatment method for a steel material according to claim 1,
wherein a treatment liquid containing an oxo acid salt of a transition metal and special modified ionized water is used in the rinsing step.

### Claim 8 (depends on 1)

The surface treatment method for a steel material according to claim 1,
wherein an oxo acid salt of a transition metal contained in the treatment liquid used in the rinsing step is either a tungstate, a molybdate, or a zirconate.

### Claim 9 (depends on 1)

The surface treatment method for a steel material according to claim 1,
wherein rustproofing of the steel material and a phosphate coating treatment are carried out simultaneously in the rustproofing step.

### Claim 10 (depends on 1)

The surface treatment method for a steel material according to claim 1,
wherein the first water washing step is repeated a plurality of times.

### Claim 11 (depends on 1)

The surface treatment method for a steel material according to claim 1,
wherein ultrasonic waves or a spray is used in the second water washing step.

### Claim 12 (depends on 1)

The surface treatment method for a steel material according to claim 1, further comprising:
a coating step of subjecting the steel material to a coating treatment.

### Claim 13 (depends on 12)

The surface treatment method for steel material according to claim 12, further comprising
producing a machine component with the steel material following the coating step.

### Claim 14 (depends on 13)

The surface treatment method for a steel material according to claim 13, wherein
the machine component is a hydraulic line for a hydraulic excavator.
