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US 2014/0212626 A1Published application
Method of making inorganic, metal oxide spheres using microstructured molds
Assignee3M Innovative Properties Company
InventorsDavid C. Kramlich, John L. Vandenberg, Matthew H. Frey, Scott R. Culler, Kathleen M. Schakel-Carlson
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Abstract
A process for making inorganic, metal oxide spheres that includes exposing solidified, molded microparticles that include a glass precursor composition to a temperature sufficient to transform the molded microparticles into molten glass and cooling the molten glass to form inorganic, metal oxide spheres.
Claims30
A process for making inorganic, metal oxide spheres, the process comprising:
- forming a glass precursor composition comprising glass precursor particles dispersed in a vehicle such that the composition forms a dispersion, the vehicle including at least one of water, an organic liquid, and a binder;
- positioning the glass precursor composition in a plurality of mold cavities;
- solidifying the glass precursor composition in the plurality of mold cavities to form solidified, molded microparticles;
- demolding the solidified, molded microparticles from the plurality of mold cavities;
- exposing the solidified, molded microparticles, after demolding, to a temperature sufficient to transform the molded microparticles into homogeneous molten droplets;
- and
- cooling the homogeneous molten droplets to form inorganic, metal oxide spheres.
4 more elements
Dependencies are inferred from the claim text.