# US 2014/0151273 A1 · Probe arrangement for a flotation cell > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 2014/0151273 A1 - Document ID: US20140151273A1 - Status: Published application - Kind: A1 - Application number: 14/239,197 - Filed: 2011-08-18 - Published: 2014-06-05 - Earliest claimed: 2011-08-18 - Assignees: Outotec Oyj - Inventors: Anssi Lehikoinen; Marko Vauhkonen - Web page: https://patentgrep.com/patent/US20140151273A1 ## CPC - G01N 27/04: by investigating resistance - B03D 1/02: Froth-flotation processes - B03D 1/028: {Control and monitoring of flotation processes; computer models therefor} - G01F 23/0023: {with a probe suspended by a wire or thread (with floats G01F23/40)} - G01F 23/242: {Mounting arrangements for electrodes} - G01F 23/245: {with a probe moved by an auxiliary power, e.g. meter, to follow automatically the level} - G01F 23/26: by measuring variations of capacity or inductance of capacitors or inductors arising from the presence of liquid or fluent solid material in the electric or electromagnetic fields - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) - B03D: FLOTATION; DIFFERENTIAL SEDIMENTATION (sedimentation in general B01D21/00; in combination with other separation of solids B03B; sink-float separation B03B5/28; detergents, soaps C11D) - G01F: MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME ## Abstract The flotation process is widely used in mineral industry for the separation of minerals from low-grade ore slurry. Several parameters, such as the bubble size distribution and/or amount of solids in the froth and slurry affect the outcome of the flotation process. To be able to monitor these parameters, knowledge of the temporal changes of froth-slurry phase interface as well as froth-air interface is essential. In the present invention, an electrical resistance tomography probe sensor, which is capable of analyzing the properties of froth and slurry based on the correlation between the estimated conductivity information and the parameters of interest, is introduced. ## Claims ### Claim at position 1 1-24. (canceled) ### Claim 25 A method, comprising analyzing material in a container comprising slurry and/or froth and/or gas and/or a transitional area between the froth and the slurry, using at least one probe comprising together a plurality of electrodes capable of being in contact with the material, the analyzing further comprising: a. injecting currents or voltages through at least two electrodes; b. measuring voltages or currents, respectively, through the electrodes; and c. determining conductivity distribution for the material using model based calculations, which comprise reconstruction of a vertical conductivity profile among the material. ### Claim 26 (depends on 25) The method according to claim 25, further comprising one or more of: determining properties of the material based on the voltage or current measurement results, the properties comprising at least one of bubble size distribution, amount of solid materials in the froth and/or slurry, and stiffness of the froth, estimating interface levels between froth-slurry and/or froth-gas interfaces and/or between the transitional area and froth and/or between the transitional area and slurry, estimating the slurry-froth interface level and/or the froth-gas interface level by a step-like change in the conductivity value of the interface, and estimating the density of the froth and/or the slurry, the density being proportional to the conductivity of the froth and/or the slurry. ### Claim 27 (depends on 25) The method according to claim 25, further comprising: detecting electrodes locating in the gas, when the measured voltage or current by these electrodes is bound by a supply voltage of the system, or when the measured voltage is beyond an allowed measurement voltage range. ### Claim 28 (depends on 26) The method according to claim 26, wherein the method is applied in a froth flotation process and the method further comprises: controlling the froth flotation process based on at least one of the bubble size distribution, amount of solid materials in the froth and the slurry, stiffness of the froth and the interface levels between froth-slurry and/or froth-gas. ### Claim 29 (depends on 28) The method according to claim 28, wherein: the controlling step is realized by at least one of adding at least one additive material changing the stiffness of the froth, choosing rate of input material feed, choosing rate of aeration, and changing parameters of grinding. ### Claim 30 (depends on 25) The method according to claim 25, further comprising: monitoring contamination of the electrodes by measuring contact impedances between each electrode and the material to be analyzed. ### Claim 31 (depends on 25) The method according to claim 25, further comprising: using in the analysis visual inspection data taken by a video camera. ### Claim 32 (depends on 25) The method according to claim 25, further comprising: measuring temperature with the at least one probe; and compensating conductivity values based on the measured temperature value. ### Claim 33 A system for analyzing material, comprising: a probe arrangement of at least one probe comprising together a plurality of electrodes capable of being in contact with the material in a container comprising slurry and/or froth and/or gas and/or a transitional area between the froth and the slurry; a current source configured to inject currents or voltages through at least two electrodes; measuring means configured to measure voltages or currents, respectively, through the electrodes; and a processor configured to control the measurements, the processor being further configured to: determine conductivity distribution for the material using model based calculations, which comprise reconstruction of a vertical conductivity profile among the material. ### Claim 34 (depends on 33) The system according to claim 33, wherein the processor is further configured to: determine properties of the material based on the voltage or current measurement results, the properties comprising at least one of bubble size distribution, amount of solid materials in the froth and/or slurry, and stiffness of the froth. ### Claim 35 (depends on 33) The system according to claim 33, wherein the processor is further configured to: estimate interface levels between froth-slurry and/or froth-gas interfaces and/or between the transitional area and froth and/or between the transitional area and slurry. ### Claim 36 (depends on 33) The system according to claim 33, wherein the processor is further configured to: estimate the slurry-froth interface level and/or the froth-gas interface level by a step-like change in the conductivity value of the interface. ### Claim 37 (depends on 33) The system according to claim 33, wherein the processor is further configured to: estimate the density of the froth and/or the slurry, the density being proportional to the conductivity of the froth and/or the slurry. ### Claim 38 (depends on 33) The system according to claim 33, wherein the processor is further configured to: detect electrodes locating in the gas, when the measured voltage or current by these electrodes is bound by a supply voltage of the system, or when the measured voltage is beyond an allowed measurement voltage range. ### Claim 39 (depends on 35) The system according to claim 35, wherein the system is applied in a froth flotation process and the processor is further configured to: control the froth flotation process based on at least one of the bubble size distribution, amount of solid materials in the froth and the slurry, stiffness of the froth and the interface levels between froth-slurry and/or froth-gas. ### Claim 40 (depends on 39) The system according to claim 39, wherein the controlling step is realized by at least one of adding at least one additive material changing the stiffness of the froth, choosing rate of input material feed, choosing rate of aeration, and changing parameters of grinding. ### Claim 41 (depends on 33) The system according to claim 33, wherein the measuring means are further configured to: monitor contamination of the electrodes by measuring contact impedances between each electrode and the material to be analyzed. ### Claim 42 (depends on 33) The system according to claim 33, wherein the system further comprises: a video camera configured to take visual inspection data for use in the analysis. ### Claim 43 (depends on 33) The system according to claim 33, wherein the system further comprises: a temperature probe configured to measure temperature and connected to the at least one probe; and the system is further configured to compensate conductivity values based on the measured temperature value. ### Claim 44 A computer program stored in a computer-readable medium, the computer program comprising code adapted to control the following steps, when executed on a data-processing system for analyzing material in a container comprising slurry and/or froth and/or gas and/or a transitional area between the froth and the slurry, using at least one probe comprising together a plurality of electrodes capable of being in contact with the material: a. injecting currents or voltages through at least two electrodes; b. measuring voltages or currents, respectively, through the electrodes; and c. determining conductivity distribution for the material using model based calculations, which comprise reconstruction of a vertical conductivity profile among the material.