Adhesive compostion
AssigneePowers Products III, LLC
InventorJames E. Surjan
Life of this patent
Estimating the term…
Abstract
An adhesive composition includes a first part comprising about 15 to about 60 wt % of an epoxy compound, about 35 to about 80 wt % of an epoxy novolac, and about 5 to about 25 wt % of an epoxy-based reactive diluent based on the total weight of epoxy compound, epoxy novolac, and reactive diluent; and a second part comprising less than about 20 wt % of a hydroxyaromatic solvent, about 80 to about 99 wt % of a Mannich base, and about 1 to about 20 wt % of a tertiary amine, based on the total weight of hydroxyaromatic solvent, Mannich base, and tertiary amine, the first and second parts being present in a volume ratio of about 0.8:1 to about 1.2:1. Additives to further enhance the properties may be included. A method of forming an adhesive layer includes applying the adhesive composition to a surface.
Claims21
An adhesive composition comprising:
- a first part comprising
- about 15 to about 60 wt % of an epoxy compound,
- about 35 to about 80 wt % of an epoxy novolac, and
- about 5 to about 25 wt % of an epoxy-based reactive diluent
- based on the total weight of epoxy compound, epoxy novolac, and reactive diluent;
- and
- a second part comprising
- less than about 20 wt % of a hydroxyaromatic solvent,
- about 80 to about 99 wt % of a Mannich base, and
- about 1 to about 20 wt % of a tertiary amine,
- based on the total weight of hydroxyaromatic solvent, Mannich base, and tertiary amine,
- the first and second parts being present in a volume ratio of about 0.8:1 to about 1.2:1.
The adhesive layer of claim 20, wherein the cure product forms after combining the first and second parts.
An adhesive composition comprising:
- a first part comprising
- about 10 to about 50 wt % of an epoxy compound,
- about 20 to about 70 wt % of an epoxy novolac,
- about 5 to about 20 wt % of an epoxy-based reactive diluent, and
- about 10 to about 40 wt % of first part additives,
- based on the total weight of the first part;
- and
- a second part comprising
- less than about 10 wt % of a hydroxyaromatic solvent,
- about 10 to about 30 wt % of a Mannich base, and
- about 0.1 to about 10 wt % of a tertiary amine, and
- about 60 to about 90 wt % of second part additives,
- based on the total weight of the second part,
- the first and second parts being present in a volume ratio of about 0.8:1 to about 1.2:1.
A method of forming an adhesive layer comprising:
- combining a first part and a second part of an adhesive composition, the first part comprising:
- about 15 to about 60 wt % of an epoxy compound,
- about 35 to about 80 wt % of an epoxy novolac, and
- about 5 to about 25 wt % of an epoxy-based reactive diluent
- based on the total weight of epoxy compound, epoxy novolac, and reactive diluent;
- and
- the second part comprising
- less than about 20 wt % of a hydroxyaromatic solvent,
- about 80 to about 99 wt % of a Mannich base, and
- about 1 to about 20 wt % of a tertiary amine,
- based on the total weight of hydroxyaromatic solvent, Mannich base, and tertiary amine,
- the first and second parts being present in a volume ratio of about 0.8:1 to about 1.2:1;
- and
- applying the adhesive composition to a surface.
A method of making an epoxy adhesive, comprising:
- forming a first combination by combining until homogeneous:
- about 23.50 wt % of bisphenol A diepoxy,
- about 43.01 wt % of epoxy novolac,
- about 9.81 wt % of 2-ethyl-2-hydroxymethyl-1,3-propanediol copolymer with chloromethyloxirane,
- about 2.51 wt % of fumed silica suspension agent,
- about 0.10 wt % of titanium dioxide,
- about 5.27 wt % of silica sand having a mesh size greater than 50, and
- about 15.80 wt % of silica sand having a mesh size of less than 25;
- forming a second composition by combining until homogeneous:
- about 24.40 wt % of 1,3-(N,N-dimethylaminomethyl) benzene,
- about 2.80 wt % of tertiary amine hardener,
- about 2.80 wt % of benzyl alcohol,
- about 0.90 wt % of fumed silica suspension agent,
- about 0.02 wt % of carbon black,
- about 17.50 wt % of fine silica sand of greater than 50 mesh, and
- about 52.48 wt % of coarse silica sand of less than 25 mesh;
- and
- combining the first and second compositions in a ratio of about 1:1 by volume.
Dependencies are inferred from the claim text.