Preparing polyester alcohols
AssigneeBASF SE
InventorsHermann Graf, Ulrike Mahn, Stefan Käshammer, Günter Scherr, Christian Nitschke
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AssigneeBASF SE
InventorsHermann Graf, Ulrike Mahn, Stefan Käshammer, Günter Scherr, Christian Nitschke
Estimating the term…
A process for preparing polyester alcohols by condensation of polytetrahydrofuran with aromatic dicarboxylic acids and/or their anhydrides and/or their esters, preferably isophthalic acid, phthalic acid and terephthalic acid and more preferably isophthalic acid, in the presence of a transesterification catalyst in a multi-stage operation at different pressure levels with at least one reaction stage at atmospheric pressure and at least one reaction stage at reduced pressure, where distillate is removed from the reaction system, comprises deactivating the catalyst after the polycondensation by using phosphoric acid in a molar ratio of 1:1 to 1:3.5 for catalyst to phosphoric acid.
1-10. (canceled)
A process for preparing polyester alcohols by condensation of polytetrahydrofuran with aromatic dicarboxylic acids and/or their anhydrides and/or their esters in the presence of a transesterification catalyst in a multi-stage operation at different pressure levels with at least one reaction stage at atmospheric pressure and at least one reaction stage at reduced pressure, where distillate is removed from the reaction system, which process comprises deactivating the catalyst after the polycondensation by using phosphoric acid in a molar ratio of 1:1 to 1:3.5 for catalyst to phosphoric acid.
Dependencies are inferred from the claim text.