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US 2012/0056341 A1Published application
Silica nanocapsules from nano-emulsions obtained by phase inversion
AssigneeYissum Research Development Company of the Hebrew University of Jerusalem
InventorsShlomo Magdassi, David Avnir, Liat Spernath
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Abstract
Silica nanocapsules are prepared from a nanoemulsions obtained by a phase inversion method.
Claims21
1-41. (canceled)
A process for the manufacture of silica nanocapsules, said process comprising:
- obtaining a nanoemulsion of an aqueous phase and an oil phase and at least one surfactant, the nanoemulsion being formed by the process comprising:
- (i) forming an oil-in-water (O/W) emulsion of an aqueous phase and an oil phase comprising at least one hydrophobic material and at least one silica precursor in the presence of at least one surfactant,
- (ii) heating the O/W emulsion above its phase inversion temperature (PIT) to obtain a water-in-oil (W/O) emulsion, and
- (iii) cooling the W/O emulsion below the PIT temperature, thereby forming a nanoemulsion of oil droplets in water;
- inducing interfacial polymerization of the silica precursor around the oil droplets in the nanoemulsions thereby obtaining said silica nanocapsules.
2 more elements
Dependencies are inferred from the claim text.