Back to results
US 2010/0249442 A1Published application
Continuous method for the heterogenically catalyzed esterification of fatty acids
AssigneeBayer Technology Sevices GmbH
InventorsDieter Heinz, Leslaw Mleczko, Shaibal Roy, Heinrich Morhenn, Wulf Dietrich
Life of this patent
Estimating the term…
Abstract
Continuous method for the esterification of free fatty acids in plant and animal fats with alcohols using a heterogenic acid catalyst.
Claims20
Continuous process for esterifying free fatty acids present in starting materials, comprising the steps of
- 1) removing the free fatty acids from the remaining starting material by means of a customary deacidification process,
- 2) optionally reacting the deacidified starting material remaining after step 1) in the form of a transesterification to obtain fatty acid alkyl esters,
- 3) reacting the free fatty acids with alcohols using at least one acidic catalyst in a fixed bed, in the form of an esterification reaction,
- 4) optionally removing the water formed as a by-product in step 3), optionally together with at least a portion of the alcohol unconverted in step 3),
- 5) optionally further converting the dewatered product obtained from step 4), optionally with addition of further alcohol, using at least one acidic catalyst in a fixed bed, in an esterification reaction,
- 6) mixing the reaction product obtained from step 3) and/or the reaction product optionally obtained from step 5) with the remaining starting material obtained from step 1) and/or the fatty acid alkyl esters obtained from step 2).
3 more elements
Process according to further comprising removal of the water formed as a by-product in step 3), optionally together with at least a portion of the alcohol unconverted in step 3).
Dependencies are inferred from the claim text.