# US 2010/0166944 A1 · Method for determining the polyester fraction of a multi-component powder during a thermal spraying process, method for coating or touching up an object by means of a thermal spraying process and thermal spraying device

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- Number: US 2010/0166944 A1
- Document ID: US20100166944A1
- Status: Published application
- Kind: A1
- Application number: 12/514,989
- Filed: 2007-11-02
- Published: 2010-07-01
- Earliest claimed: 2006-11-15
- Assignees: MTU Aero Engines AG
- Inventors: Andreas Jakimov; Manuel Hertter; Andreas Kaehny
- Web page: https://patentgrep.com/patent/US20100166944A1

## CPC

- C23C 4/04: characterised by the coating material
- C23C 4/12: characterised by the method of spraying
- G01N 21/00: Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light (G01N3/00 - G01N19/00 take precedence)
- G01N 21/71: thermally excited
- G01N 21/73: using plasma burners or torches
- G01N 2021/8416: {and process controlling, not otherwise provided for}
- C23C: COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL (making metal-coated products by extrusion B21C23/22; covering with metal by connecting pre-existing layers to articles, see the relevant places, e.g. B21D39/00, B23K; metallising of glass C03C; metallising mortars, concrete, artificial stone, ceramics or natural stone C04B41/00; enamelling of, or applying a vitreous layer to, metals C23D; treating metal surfaces or coating of metals by electrolysis or electrophoresis C25D; single-crystal film growth C30B; by metallising textiles D06M11/83; decorating textiles by locally metallising D06Q1/04)
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

A method for determining the polyester fraction in a multi-component powder during a thermal spraying process is disclosed. The multi-component powder is heated and fed to an object with the aid of a carrier, forming a coating on the object. At least one measured value for the intensity of the light emitted by the combination of the carrier and multi-component powder material on the way to the object is detected at least in the range of a characteristic wavelength of polyester. A characteristic value is derived from the combination of the measured values, and the fraction of the polyester to be determined is calculated on the basis of a previously determined relationship between the characteristic value and the polyester fraction.

## Claims

### Claim at position 1

1-13. (canceled)

### Claim 14

A method for determining a polyester fraction in a multi-component powder during a thermal spraying process, comprising the steps of heating and feeding the multi-component powder to an object with aid of a carrier, forming a coating on the object, and measuring a first value for an intensity of light emitted by the carrier and measuring a second value for an intensity of light emitted by a combination of the carrier and the multi-component powder, deriving a characteristic value from a comparison using the first and second measured values, and determining a fraction of polyester in the multi-component powder on a basis of a previously determined relationship between the characteristic value and the polyester fraction.

### Claim 15 (depends on 14)

The method according to claim 14, wherein the first and second measured values are both recorded in a first predetermined wavelength range around a characteristic emission wavelength of polyester and in a second predetermined wavelength range that does not overlap with the first wavelength range around a characteristic emission wavelength of a material of the multi-component powder other than polyester, and, on a basis of the first and second measured values the characteristic value is formed as a relative quantity.

### Claim 16 (depends on 15)

The method according to claim 15, wherein the first predetermined wavelength range extends from 370 nm to 392 nm.

### Claim 17 (depends on 15)

The method according to claim 15, wherein the multi-component powder is comprised of polyester and a binding agent and wherein the second predetermined wavelength range extends from 392 nm to 400 nm.

### Claim 18 (depends on 14)

The method according to claim 14, wherein the step of deriving a characteristic value from a comparison using the first and second measured values includes comparing a difference of the first and second measured values.

### Claim 19 (depends on 19)

A method for coating or touching up an object by a thermal spraying process, wherein the process includes the method of claim 19 and further comprises, during the thermal spraying process, the fraction of polyester is determined multiple times or constantly, and regulated to a predetermined value or range of values.

### Claim 20 (depends on 19)

The method according to claim 19, wherein, separate from a device for the thermal spraying process, the multi-component powder is mixed from at least polyester and coating material in a mixing device directly prior to being fed to the device for the thermal spraying process, and wherein a supply of polyester and/or coating material in the mixing device is regulated during generation of the multi-component powder.

### Claim 21 (depends on 19)

The method according to claim 19, wherein a device for the thermal spraying process is used which is fed the multi-component powder from a container previously filled with the multi-component powder and wherein the fraction of polyester is regulated by spray parameters.

### Claim 22 (depends on 19)

The method according to claim 19, wherein a turbine part or engine part is coated.

### Claim 23 (depends on 19)

The method according to claim 19, wherein the thermal spraying process is plasma spraying.

### Claim 24

A device for a thermal spraying process, comprising a first feed device for a first ingredient of a multi-component powder and a second feed device for a second ingredient of the multi-component powder, wherein the ingredients fed from the two feed devices are mixed at a location of the device such that the ingredients from the two feed devices mix when the device is in operation and before the multi-component powder impacts an object to be coated by a thermal spraying process.

### Claim 25 (depends on 24)

The device according to claim 24, wherein the first and second ingredients are heated in the device.

### Claim 26 (depends on 24)

The device according to claim 24, wherein at least one of the feed devices is controlled by a regulating device which analyzes signals of an optical spectrometer.
