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US 2010/0062271 A1Published application
Process for producing improved binders for plastisols
AssigneeEvonik Roehm GmbH
InventorsJan Hendrik Schattka, Gerd Loehden, Winfried Belzner, Ulrike Behrens, Christian Golditz, Sebastian Grimm, Herbert Jung, Florian Matthes
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Abstract
The invention relates to a process for preparing binders for plastisols that ensures high and consistent product quality over a multiplicity of batches. The binders obtained from this process allow the formulation of plastisols which possess improved stability on storage and, after gelling, improved mechanical properties.
Claims33
Process A process for preparing a binder for plastisols, characterized in that wherein
- first of all a polymer dispersion A is prepared whose particles are not larger than 200 nm,
- then a portion of dispersion A, together where appropriate with additional water and/or additives or auxiliaries, is charged to a reactor and
- a monomer or a monomer mixture
- where the monomer or each monomer has a water-solubility of in each case more than 0.01% by weight at 20° C.,
- together where appropriate with water, emulsifier or other admixtures, is metered into this reactor and polymerized therein in such a way that the average size of the particles rises by at least 50 nm, and then
- where appropriate, one or more further monomers or monomer mixtures,
- which are different from the first monomer or first monomer mixture, and where, again, the monomer or each monomer has a water-solubility of in each case more than 0.01% by weight at 20° C.,
- together where appropriate with water, emulsifier or other admixtures, are metered into this reactor and polymerized therein in such a way that the average size of the particles rises in each case by at least 50 nm, and
- then the resulting dispersion B is spray-dried to give a powder which, as it is or, where appropriate, after complete or partial grinding, constitutes the binder.
6 more elements
Dependencies are inferred from the claim text.